ࡱ > . 0 ) * + , - 3 4 5 6 7 8 i 9 R bjbj xA l n n n 8 n Dt . Lx Lx " nx nx x ?z ?z ?z ` b b b b b b $ B ?z z " ?z ?z ?z nx x [ ?z / R nx x ` ?z ` l D " x @x p8Bb xl n S X & d q 0 & 1 B 1 ,{1 2 z SP[8T6eIQ1Rg(WwlS]T{]W-Nv^(u
1 2 . 1 i
1 2 . 2 SlSvQ RekR]NTvRg
1 2 . 2 . 1 7hTMRYti
1 2 . 2 . 1 . 1 vcۏ7hKm[
1 2 . 2 . 1 . 2 7hTve:gSYt
1 2 . 2 . 1 . 3 Rge^lavQ*N
1 2 . 2 . 2 7hTRg
1 2 . 2 . 2 . 1 SlT͑l-N_ϑCQ }Km[
1 2 . 2 . 2 . 2 {l-N_ϑCQ }Km[
1 2 . 2 . 2 . 3 mnl-N_ϑCQ }Km[
1 2 . 3 S]irT-N_ϑCQ }vRg
1 2 . 3 . 1 7hTMRYti
1 2 . 3 . 2 7hTRg
1 2 . 3 . 2 . 1 ;m'`p[ƖKm[YNpl-Nv7x+Tϑ
1 2 . 3 . 2 . 2 Tbh-N_ϑCQ }vKm[
1 2 . 3 . 2 . 3 aj-N_ϑCQ }vKm[
1 2 . 3 . 2 . 4 me-N_ϑCQ }vKm[
1 2 . 3 . 2 . 5 ZoNTSvQSe-N_ϑCQ }vKm[
1 2 . 4 PSBR0mRBRT|~S]NTvRg
1 2 . 4 . 1 7hTMRYti
1 2 . 4 . 2 7hTRg
1 2 . 4 . 2 . 1 PSBR-N_ϑCQ }vKm[
1 2 . 4 . 2 . 2 mRBR-N_ϑCQ }vKm[
1 2 . 4 . 2 . 3 |~S]NT-N_ϑCQ }vKm[
1 2 . 5 SYT-N_ϑCQ }vRg
1 2 . 5 . 1 7hTMRYti
1 2 . 5 . 2 7hTRg
1 2 . 5 . 2 . 1 8^(uSYT-Nv_ϑCQ }Km[
1 2 . 5 . 2 2 mSmSYr-N_ϑCQ }vKm[
1 2 . 6 vQ[S]SeTNT-N_ϑCQ }vRg
1 2 . 6 . 1 7hTMRYti
1 2 . 6 . 2 7hTRg
1 2 . 6 . 2 . 1 S]Se-N_ϑCQ }Km[
1 2 . 6 . 2 . 2 vtstSvQSe-N_ϑCQ }vKm[
1 2 . 6 . 2 . 3 vQNS]NT-N_ϑCQ }Km[
,{1 2 z SP[8T6eIQ1Rg(WwlS]T{]Wv^(u
1 2 . 1 i
1 9 5 5 t^, W a l s h cQSP[8T6eIQ1SN\O:N N,Rgel^(u[ 1 ] 01 9 6 1 t^, R o b i n s o n [ 2 ] TS p r a g u e [ 3 ] I{NR+RcQNSNvcb(unBR zʑT(uSP[8T6eIQ1Rg}llTmnl7hT01 9 6 7 t^B a r r a s I{N(W,{7 J\NLuwlO
NbJTNNNv
0SP[8T6el(Wwl]N
Nv^(u 0~e[ 4 ] 0@wSP[8T6eIQ1b/gvSU\TnfS, [(WSl0-NNirT g~NT-N_ϑCQ }vRgeb_0RN^lv^(u0vQ-N NNSP[8T6eIQ1Rgel, ]b:NVA S T M TVE
N(uvhQRgel0(WbV, SP[8T6eIQ1Rg~Ǐ NASYt^egvSU\, ]nfS0RSbwlS]T{]LN(WQvVl~NmvT*NW;5 ^9 =, vQ-N] g
N\SP[8T6eIQ1RgelR:NLNTV[hQRgel0
wlS]T{]7hT y{|A~Y0egn
YBg
N T7hT'`(]+R_'Y0e gm`, _N gV`0l`e g g:gir, _N ge:gir0Sl0mnl|^_'Y, wl0}llQNNY T4lr, Nwl7hTf%cS, fqfr, lww0PSBR0mRBRI{S^8^3zV07hTegnTy{|vY7h'`, bN7hTYtT6R7helvY7h'`, Te_N:NgN7hTvYt&^egvS_'YvV0
(WwlS]T{]v uNǏ z-N, NSPge6e0-N uNǏ zv(ϑc6R0RNTQShvTs, TSNO(uSP[8T6eIQ1lv0We_Y0vMRNSl-Nt[Qvё^\N^ё^\CQ }~ NASYy, ;N gF e 0N a 0M g 0 N i 0 V 0 C a 0P b 0M o 0M n 0C r 0C o 0B a 0Z n 0K 0A s 0A l 0B 0Z r 0P d 0C d 0S i I{0bVSl-N V +TϑY:NQ*Nm g . k g - 1 , N i +TϑRؚQ~vm g . k g - 1 0(Wwlp6RR]-N, ё^\+TϑvY\/fċNpl]zSvQNT(ϑv͑ch;1 0 = vQ-NgNё^\/fwlR]Ǐ z-NASR g[vBg(( Y: A s 0N i 0V ) 0
l7h-Nё^\CQ };N g Nyegn: ( 1 ) )Y6qX[(WNwl-Nvё^\2 wl _Ǒ0R]PЏS(WwlNTO(uǏ z-Nvё^\alg, YYvP0x_c, [ё^\ۏeQwlNT3 NmRBRe_ۏeQlT-Nvё^\bR, ;N/f:NN9eUwlNTvO(u'`, Ymnl-NmR g:gё^\STir, Sw0R2P0b'lS0bx0bSI{\O(u}ll-NmRpWŔSTirbN02uWs
bNp NW0M M T I{ё^\STir, ScؚvQbr'`Ulޘ:gqel-NmR g:g0STir/f:NNmdޘ:gvSu0{]NT-Nvё^\W,g
NegꁎNSe0mRBRTvQR]Ǐ z0
(WwlSvQR]NTRg-N, RgvY/f g:gir-Nve:gё^\CQ }, NCQ }+TϑVؚNO
N N, ]+R_'Y0'YYpeё^\CQ }
NvcnNwlTwl7hT, O(uё^\ g:gSTirM6R7hT, ُ:Nh7hM6RTRg~gvQnx!hck&^eg
N\V0wlSvQR]NT, Y:Nf%cS0fqT gkirT, ُ_NO~Rg&^egY0
1 2 . 2 SlSvQ RekR]NTvRg
1 2 . 2 . 1 7hTMRYti[ 1 0 ^1 7 ]
9hnclTv|^0[^I{'`(, S\l{|7hTRb͑lT{l$N'Y{|0͑l;NSb: Sl0lR0#nl0mnl0͑v( R> 3 0 0 !) PSSSelI{, ُ{|7hT|^'Y, (0lR(Y0{l;NSb: gl0}ll0wl0͑teSel0nBRlI{0ُ{|7hT|^\0R{, ,gё^\+TϑNO, FO(WbTlR]Ǐ z-N, ge ReQmRBR _ۏgNё^\0lT-Nvё^\+TϑRgelbq, e.sY Yel]b:NLNhQRgel0,g c͑l0{l0mnl N{|R+RN~vQRgel0
SP[8T6eIQ1Rgwl7hT, MRYtǏ z/fQ[Rg ^vsQ.0YtelR:N$N{|;1 0 , 1 1 = N/f g:girvcۏ7hKm[ N/fۏLe:gS sS\ g:girdS \Kmё^\lS:Ne:gv{|KNTۏLKm[0MROp/f7hTYtk{USeO, Rg ^_0:p/f g:gё^\STirh7hegnS0RP6R, ~gvQnx!hckX[(WV0TvOp/fS7hϑup;m, YtǏ z g N[v[Ɩ\O(u, hQPk g:girvcۏ7hNO /f^(u geT g^lvel0:p/fMRYt9e0'Y Km~R"N1YTSalgvS'`XR0
1 2 . 2 . 1 . 1 vcۏ7hKm[
vcۏ7hKm[/f\l7hvcbO(u N[v g:gnBRmTT, vcۏ7hNkp0qbwXpSP[ShVۏLKm[vel0
1 . wXpvcۏ7h
{l|^\, Svcۏ7hNwXpSP[ShVQ͑lT|^'Yvl7h, (uTvnBR( Y: 2uW_NWn0V"lKTU0N2u0nBRlI{ zʑTۏ7h0
vcۏ7hKm[e, g}YReQS_vWSO9eۏBR, N2bkKmCQ }(WppS6k_c1Y, v^KQ
gVCQ }b_`
N T@b bvupOe^]_0Y: ReQ]xxAO2kKmCQ }Sb]xxvbё^\~TirRxOTypWŔSbxŔ~TirI{0=\{wXpvcۏ7hKm[ gvQ
NKNY FO1uNRg ^_ N g N[[(uNeQvS_N {k҉ X[ϑv3 ~ 5
PT, Ǒ7hN[hV-N, zsSRv0Pf0lnS7he, (uN蕄vS7h]wQ, (WPv
N0-N0 N
N TMOS7hmTsSS0S7hT=\_Rg, 2bkgQ|P[0lm0IQSZTI{S^S u0
2 . MQ7hTalg
7hT-Nё^\CQ }Y:Nuϑ4ls^, ge (uwXplb"lSirS ulRg0^la7hT[hVbSf[ՋBRalg0YvǏ+TŔ}llv[hVQňwl,
Nlanm, 1\algwl0 TeRg@b(uՋBR=\ϑ(u~^ؚvO~~0IQ1~ՋBR, NMNOzz}v
e_wRg~gOPNO0a$ppS_c1Y0ppS)n^Ǐؚbfkpqpepl_c1Y0@bNppSe[
N T7hT,
N TCQ }R N[vppSRBR, Tec6RppS)n^/f_ v0b$xmS
N[hQ0l7h-NvYё^\STirNkSObrV~T, bKmCQ }NkSO[hQRy
N_[f, Vdk(WxmSe, (uTvxmSBR0'lSBR, v^S_XRxmS!kpe0c$[hVv8TD0@b(uvstNhV0QXet[gNCQ }( Y: A s ) g N[v8TD\O(u, S7hT^=\_KmՋ0
4 . g:gnBRvq_T
N g:gv\O:NKmՋnmNe:g4lnmvk g'Yv]+R0 g:gnBRqpefyp fPNhVQXeN qp ^SS'Y0^yr+RlaN NQp`$Senmkp0qSP[ShV0 _YHQ8TUYNnmnmSP[ShV, Q8TUՋ7h~_gKm[e HQ8TUzz}v g:gv, Q8TUYNnmnmSP[ShV0a$T bqRk Ockp0qqpr`3z[0b$laNhVv0 (uTv g:gnBR\O:Nzz}vՋBR Nzz}v0hQ07hT(u Ty g:gnBRTv TkOvW@xlM6R0c$RgǏ z-NO(uN蕄v^mcl{ST^m80d$ gNNhV( YP e r k i n - E l m e r |Rv'YRNhVI{) S[+gz[\Wbcb(g(W, wXpꁨRۏ7hhVRMN_Nfbc, N2 g:gnBRPQXeMN, q_TNhVvO(u[}T0
1 2 . 2 . 2 7hTRg
1 2 . 2 . 2 . 1 SlT͑l-N_ϑCQ }Km[
1 . wl7hT-N7x+TϑKm[
(uM I B K zʑwl7hT, zʑk:Nl: zʑBR= 1 : 3 ( v / v ) 0(W1 0 m L Rmoe-NO!kReQ N[ϑv zʑTl7hT5 0 g . L - 1 vI 2 - 2unm;2 1 =, /caT>en1 m i n , QReQ2 m L 1 H N O 3 , S1 m i n , RB\T\ NB\4lvly0R2 0 m L pog-N0͑
YS N!k04lvN5upg
NRpr^0QtSTNpog-NQnxReQ2 m L 1 H N O 3 , (u_ϑS7hhVRSVN( kN2 0 0 L ) N1 m L Ջ7hog-N0R+RReQ0 01 0 02 0 03 0 L 1 m g . L - 1 vA s hm (u4l z4 0 0 L 0
Rg~l:N1 9 3 . 7 n m &^[^2 . 6 n m ؚ'`zz_4gopop5uAm7 . 5 m A 0pwX{0ۏ7hϑ2 0 L 0wXp)n^ z^: r^q1 2 0 !, Oc1 5 s ppS1 2 0 0 !, Oc2 0 s SP[S2 8 0 0 !, Oc4 s QS2 9 0 0 !, Oc3 s 0}lAmϑ2 0 0 m L . m i n - 1 0Kmϑe_:N\ؚ hQReQl[ϑ0WSO9eۏBRP d C l 2 Sm^:N1 0 g . L - 1 ( NP d ) , ReQk:N P d : A s = 8 0 : 1 ( m / m ) 0
S_nm-NM n 0A l 0V 0B 0P v(ϑSm^R+R:N6 03 02 5 01 0 0 01 3 m g . L - 1 e, [A s Km[ gckr^pbC r 0C o 0W 0M o 0C u 0F e (ϑSm^:N5 06 01 0 0 01 0 0 02 0 0 03 7 5 m g . L - 1 e, [A s Km[ g r^pb0
elvhQP( k = 3 ) :N7 . 5 g . L - 1 ~'`V/f1 3 ~ 2 5 0 g . L - 1 R S D /f2 . 8 0RhV6es/f9 8 ~ 1 0 2 ,glNnlm㉌T zʑۏ7hlKm[~g N0
laNyt$lvN4lvk:N1 : 2 [0u$ I 2 - 2unm(uϑ(W0 . 6 ~ 1 . 0 m L eq_T, ,gl(u0 . 8 m L 0v$S/caTYneGW:N1 m i n 0w$ (uNn\O zʑBR, ̀of'Y0
2 . Sl-NTMvKm[
yS N[ϑ( 1 ~ 2 g ) SlnNpog-N (u g:gnBR( _N: QYNx: s]n= 1 : 1 : 1 6 ) [hQnm0R[ϑt-N Ns]n zʑ;R^ Gd S0
vc(ukp0qSP[8T6eIQ1lKm[ F e Km[agN/fl2 4 8 . 3 n m op5uAm3 . 0 m A &^[^0 . 2 n m 0YNpAmϑ0 . 9 L . m i n - 1 , zzlAmϑ6 . 5 L . m i n - 1 0lop5uAm4 . 5 m A , h:\ibU\
Ppe 2 0Km[N i vagN/flN i 2 4 8 . 3 n m lop5uAm6 . 4 m A h:\
NibU\ vQNagN TF e vKm[0hQf~l[ϑ hQ]\Onm(ue:gvv4lnmR g:gnBRM6R0
1uNSl~b
YBg qQX[irRP[8T6eTIQ1ce\ b%N͑̀ofr^pb ǑS N[v̀of!hckce;2 2 =0(u^XfHe^cb̀of, F e 0N i s^GWRhV6esR+R:N1 0 5 T9 8 . 1 , R S D R+R:N5 . 7 T1 0 (ulopcb̀of, F e 0N i s^GWRhV6esR+R:N8 3 . 4 T8 2 . 0 , R S D R+R:N5 . 7 T1 0 0
laNy1 ReQ\ϑv_NTQYNx /f:NNOe:gnmT g:gnBRmn2 (u^XfHe^cb̀ofe_KmF e 0N i GWS_t`Heg)R(ulopcb̀ofe [F e vKm[~gt` [N i vKm[~gOPNO ُ/fV:Nlopcbd̀ofǏ^@b0
3 . sNJmmۏ7hkp0qlKm[#nl-NvM
QnxS7hT1 4 g ]SnNr^pog-N, (u\ϑmTnBRn, v^(uM I B K + N2u( 2 + 3 ) mTnBR[[1 0 0 m L [ϑt-N0Sdknm8 . 0 0 m L N5 0 m L kr{-N, ReQ6 . 0 0 m L 2 0 v / v T r i o n X - 1 0 0 nm, (u 3 5 0 !͑l0> 5 0 0 !#nlI{7hT (u]xxNvx(WSRn9_Qm㉬PSBR7hT S(uNExݔRP[[{PSBRI{7hT-N_ϑV vKm[01 0 0 0
PϑvF e 0N i 0C u 0P b 0A l 0N a 0M g
Nr^pbV vKm[0
laNy:N: 1 (unfwX{bs^S{Km[\b_[ b>\͑ (uhQpwX{02 1 0 ~ 2 0 vH C l [Km[
Nr^pb, FOx^*Y'Y, PNhV, q_TwX{v[}T0
1 2 . 2 . 2 . 2 {l-N_ϑCQ }Km[
1 . "lSirlKm[7x+Tϑ
S N[SOyvl7hnN N҉pt-N, R2 ~ 5 m L SmH 2 S O 4 , (W5upg
N\_Rp3 ~ 5 m i n , S NQtS0ޏ~GdRpe!k, lB\YeblvRS0\_nR3 0 H 2 O 2 nmerf, ~~Rp gS O 3 }vpN u, QtSTyeQ[ϑt-N, ReQpen؏SBR( 1 g K I T0 . 6 g bOW@xnN1 0 m L 4l-N) , N4l[[0nm-NvNN7x؏S:N NN7x0QReQN a B H 4 nm( 1 g N a B H 4 nN2 0 0 m L 0 . 5 N a O H nm-N) ؏SbA s H 3 , 1u}l&^eQwSP[ShVۏLSP[S;2 8 =0
Rg~lA s 1 9 3 . 7 n m zz_4gop5uAm6 m A SP[S)n^9 5 0 ! 7hTm[ϑs0 . 4 m L }Am( 5 H 2 S O 4 ) 1 0 m L . m i n - 1 N a B H 4 Amϑ1 . 2 ~ 2 . 0 m L . m i n - 1 0}l( A r bN 2 ) Amϑ1 2 0 ~ 1 8 0 m L . m i n - 1 0Kmϑe_̀of!hck( B G C ) 0(u\ؚhQf~[ϑ0
elvyr_Sm^/f0 . 2 n g . m L
1 hQP/f0 . 6 5 n g . m L
1 0,gl(uN͑teSel0wl0glI{{l-Nuϑ7xvKm[0
laNy1 wlTgl7hTvS7hSR:N: A s > 1 0 0 n g . m L
1 eS1 m L 1 0 0 ~ 4 0 n g . m L
1 eS2 m L 4 0 ~ 1 0 n g . m L
1 eS5 m L < 1 0 n g . m L
1 eS1 0 ~ 2 0 m L 2 7hTYtT^ŏ Km[5 wXplKm[S7hTYtelSSe.s[ 2 9 ]
_lmKm[}ll-Nv
_lml[ 3 0 ] QnxS2 . 5 m L }llReQmP-N 6qTReQ6 m L 6 8 % H N O 3 >eeQ_lm|~-N SR0meS_lRs ۏLm _m~_gT SQQtS ly1 0 m L [ϑt-N [[0
8^ĉYt7hTlS5 0 0 m L }llՋ7hN1 0 0 0 m L Rmoe-N ReQ2 m L x- N2u1 % op/caTR5 m L H N O 3 1 0 % /ca5 m i n YnRB\ 6eƖ NB\xmN5 0 m L pog-N Q(u5 m L H N O 3 xmS N!k gT(u1 0 m L 4lxmS N!k \xmSmTv^TN5up
NRpSpog-NxmiR2 m L ]S ly1 0 m L [ϑt-N [[0
Km[+Tϑvv[hQOP]R S D 8^ĉl:N2 . 6 1 % ~ 3 . 5 3 % _lml:N1 . 0 1 % ~ 1 . 4 5 % RhV6es8^ĉl:N9 4 . 9 % ~ 1 0 4 . 9 % _lml:N9 6 . 3 % ~ 1 0 4 . 4 % 0qQX[CQ }
Nr^pbKm[0 gsQvQNvvcۏ7hKm[SS0vel;3 1 , 3 2 =0
YNpAmϑk^'YN0
vcۏ7hkp0qlKm[}ll-N0+Tϑ;3 1 =
(u2uW_NWnM I B K nϑxx0Mb2 6 4 . 2 m g . L - 1 v0hQkm0KNT(W4 *N5 0 m L [ϑt-N R+RReQϑ0hQkmTzz}vՋBRS(u+Ŕ}llbnBRl QTvQ-NReQ0 . 1 m L n- V/lSxnm (u1 % /lS2uW NW- M I B K zʑ;R^ M6RvhQ|R:N0 . 0 0 01 3 . 2 1 02 6 . 4 2 03 9 . 6 3 m g . L - 1 0 cM6RhQ|Rnmel bhQkm9eb5 . 0 m L _Km}ll7hTM6RՋ7h0(W [vagN Nۏ:gKmՋ ~6R]\Of~ v^Km[Ջ7h+Tϑ0
NhVagNl2 7 9 . 5 n m IQ1&^[0 . 2 n m op5uAm5 . 0 m A Kmϑe3 s zzlAmϑ1 3 . 3 L . m i n - 1 YNpAmϑ1 . 7 5 L . m i n - 1 +qkp0q qp4Yؚ^1 3 . 5 m m Ǒ(ucb̀ofe_0hQf~l[ϑ0
RhV6es(W9 7 . 7 % ~ 1 0 3 . 8 % 0,gel(uN0+Tϑ(W0 . 2 5 ~ 3 0 m g . L - 1 VQ}llKm[0
laNy:N( 1 ) zz}vՋBRT}ll-Npp+Tϑ[Km[q_T'Y0(u_p\Ozz}vՋBR Km[~gOPؚ(u+Ŕ}llbnBRl\Ozz}v ~RN}llcя Km[~gS`02 ncpe(W5 0 N Ne pp[Km[~gq_T_\ ncpe'YN5 0 e Km[eQ4lv0 T7hQR+RReQ5 m L 1 0 H N O 3 nmS1 0 m L 4lTxmS1 !k03 !kxmSmTv^N1 0 0 m L pog-N, baRpiR2 m L ]Se, S NQtS, (u1 H N O 3 ly[[;3 5 =0
Rg~l:NP b 2 8 3 . 3 n m , zz_4gop5uAm1 0 m A &^[^0 . 2 n m 0lop!hck̀of0Kmϑe_:N\by0ۏ7hSOy2 0 L , WSO9eۏBR/f1 M g ( N O 3 ) 2 ReQϑ5 L , A r lAmϑ3 0 0 m L . m i n
1 SP[S6k\Pl0wXp)n^ z^:N: ppS)n^7 5 0 !, Oc3 0 s QtS0R2 0 !, Oc2 0 s SP[S)n^1 2 0 0 !, Oc3 s QS)n^ 2 6 0 0 !, Oc2 s 0(uhQf~l[ϑ0
elvR S D :N3 . 2 1 n = 6 yr_(ϑ:N1 1 p g RhV6es:N9 3 ~ 9 9 0,gl(uN(uwl-NuϑŔvRg0~xmST, qQX[CQ }
Nr^pbKm[0
^laNy:N( 1 ) @b(usthVv, ~xmmb1 0 ]xxxml( 2 ) SP[SekMR, R NQtSek, Heg}Y0
1 2 . 2 . 2 . 3 mnl-N_ϑCQ }Km[
1 . mnl-N Km[
S~0 . 1 g ĂW N2uW/lST1 g ASNpWxx, nN1 L nBRl( &{TS H 0 0 5 ĉ[) -N, v^(W9 5 5 !4ltm-NRpnb:NqTnm, Nonm\O:Nzz}vnm0(u g:gB a 0C a 0Z n vR2 - YNW]xSϑ}vlM6RhQPYm0Q(uzz}vnm zʑbhQ]\O|Rnm0yS0 . 1 g ~ 0 . 3 g Ջ7h( Qnx0 . 1 m g ) N2 5 m L [ϑt-N, (uzz}vnm z;R^;3 4 =0(uhQf~l[ϑ0Km[agNYh1 2 . 4 @b:y0
h1 2 . 4 Km[agN
CQ } l
/ n m op5uAm
/ m A IQ1&^[
/ n m qphVؚ^/ m m zzlAmϑ/ L . m i n - 1 YNpAmϑ
/ L . m i n - 1 ibU\
Ppe ՋmcSϑ
/ m L . m i n - 1 B a 5 5 3 . 5 9 0 . 9 5 7 1 0 1 . 8 5 2 . 6 C a 4 2 2 . 7 8 0 . 3 8 1 0 1 0 2 . 3 1 2 . 6 Z n 2 1 3 . 9 6 0 . 3 8 6 1 0 2 . 1 1 2 . 6
,gl(uNB a 0C a 0Z n +TϑR+R:N0 . 1 ~ 0 . 8 ( m / m ) 00 . 0 3 ~ 0 . 4 ( m / m ) 00 . 0 2 ~ 0 . 1 6 ( m / m ) *gO(uǏvmnlRg,
N(uN+TݔmRBRSYNxvmRBRvlT0
laNy:N: ( 1 ) uϑRgeSXRՋ7hϑ2 g ( Qnx0 . 1 m g ) , Te(Wh7h-NReQϑ}vl, Onm|^ N( 2 ) (WSknmTՋ7hnmKm[vGk gQ,
Ne8TUzz}vnm, NOcKmϑagNv N'`0
2 . mnlTmSOqe-NܔvvcKm[
(u g:gё^\ܔvR6 m L 2 - YNW]x0ϑ}vlM6RhQPYm0N]N(unBRl zʑhQPYmM6RhQ]\O|Rnm0\Ջ7h(W4ltm-NRp5 0 ~ 6 0 !, dbGW S, QnxyS0 . 1 ~ 0 . 3 g Ջ7h( Qnx0 . 1 m g ) nN2 5 m L [ϑt-N, (unBRl zʑ;R^;3 4 =0
Km[agN:N: lC u 3 2 4 . 7 n m , op5uAm 7 m A &^[^0 . 3 8 n m 0zzlAmϑ1 0 L . m i n - 1 , YNpAmϑ2 . 0 L . m i n - 1 , qphVؚ^5 m m 0ՋmcSϑ2 . 8 m L . m i n - 1 0(uhQf~l[ϑ0
!hQf~~'`V:N0 ~ 8 m g . L - 1 0,gl(uNmnlTmSOqe-NC u +TϑKm[0
^laNy/f: ( 1 ) h7h-NReQϑ}vl, Onm|^ N0ؚ+TϑՋ7hSNǏ9eSIQvIQ z, Q\y7hϑb zʑI{elۏLKm[0( 2 ) (WSknmTՋ7hnmKm[vGk gQ,
NeUeQzz}vnm, NOcKmϑagNv N'`0
3 . Tb*zzmnl-N_ϑё^\vvcKm[
(u3 0 0 m L YNxNoT2 0 0 m L QYNxmTGd SMbmTnBR0S2 . 5 m L 7hTnN2 5 m L [ϑt-N, (umTnBR z;R^;3 4 =, \O:N7hm0NmTnBR\O zʑBR, 1uC u 0F e 0M g 0N i 0C r 0A g ve:ghQPYmM6RhQ]\O|Rnm0vQ-NA g MbUS Nhm, vQ[MbmThm0hQ|R-N+T4lϑ
N^'YN2 0
Km[agN:N: l C u 3 2 4 . 7 n m F e 2 4 8 . 2 n m M g 2 8 5 . 2 n m N i 2 3 2 . 0 n m C r 3 5 7 . 9 n m A g 3 2 8 . 1 n m 0(u+qvzzl- YNpkp0q0vQ[agNƉNhV
N T:S+R[_0!hckf~v~'`VM g :N0 . 1 ~ 0 . 5 m g . L - 1 vQNCQ }GW:N0 . 1 ~ 1 . 0 m g . L
1 0(uhQf~l[ϑ0
,gl(uN*gO(uǏvTb*zzmnl-N_ϑё^\+TϑvKm[ 0
4 . ^(u g:ghQir(Km[mnl-NTM
yS+Tϑ:N1 0 0 g . g
1 vF e bN i hQir(;3 6 =0 . 5 0 0 0 01 . 0 0 0 0 01 . 5 0 0 0 02 . 0 0 0 0 g N2 5 m L [ϑt-N R+RReQSY(u}vl( &{TS H 0 0 0 7 Sĉ[) 0 00 . 5 01 . 0 01 . 5 g (u2 0 0 SnBRl( &{TG B 1 9 2 2 - 8 0 ĉ[) zʑ;R^0vQSm^R+R:N2 . 0 0 04 . 0 0 06 . 0 0 08 . 0 0 m g . L - 1 F e vS N|RSm^:N1 0 . 0 0 ~ 8 0 . 0 0 m g . L - 1 /fN1 0 0 0 g . g - 1 F e hQir(M6R b0zz}vl(u2 g }vlR2 0 0 SnBRl zʑ2 5 m L [ϑt-N0yS2 g 7hTN2 5 m L [ϑt-N (u2 0 0 SnBRl zʑ;R^0
Km[agN:NlF e 2 4 8 . 3 n m , N i 2 3 2 . 0 n m 0op5uAm:N1 2 m A IQ1&^[:N0 . 2 n m 0ՋmcSϑ3 . 5 m L . m i n
1 0zzlAmϑ1 0 m L . m i n
1 YNpAmϑ2 m L . m i n
1 0(uhQf~l[ϑ0
elvyr_Sm^:N F e 0 . 0 4 8 m g . L - 1 N i 0 . 0 4 4 m g . L - 1 0R S D F e :N0 . 9 2 n = 6 Sm^1 . 8 4 m g . L - 1 N i :N1 . 5 2 ( n = 6 Sm^1 . 0 0 m g . L - 1 ) 0RhV6esN i :N9 9 ~ 1 0 2 0,gl(uN}lfmnlS9(uqel-NF e 0N i vRg0
S_l-NF e (ϑSm^:N1 0 ~ 8 0 m g . L - 1 e (ulF e 3 7 3 . 7 n m SؚhQ|R6R\O!hckf~0
5 . mnl-NvKm[
Sϑ g:ghQir(nN1 0 0 m L pog-N, ReQ3 m L 2u, 7 m L 2 - YNW]xT2 0 g }vl, (W)npr` N( gؚ5 0 !) dbn, Q1 8 ~ 2 0 !T, (u}vlmR0R1 0 0 g , F e +Tϑ^:N2 0 0 m g . k g
1 0(unBRl zʑbhQ]\O|Rnm0Ջ7h)np6 0 !, dbGW S, nSv_'YN0 . 0 5 m m vVSO_|0S1 ~ 3 g ( Q0 . 1 m g ) N2 5 m L [ϑt-N, (unBRl z;R^;3 4 =0
Km[agN:N: lF e 2 4 8 . 3 n m , op5uAm9 m A , IQ1&^[0 . 1 9 n m 0zzlAmϑ1 0 L . m i n
1 , YNpAmϑ2 L . m i n
1 , qphVؚ^ 4 m m 0ՋmcSϑ2 . 8 m L . m i n
1 0(uhQf~l[ϑ !hckf~v~'`V/f1 ~ 5 m g . L - 1 0,gl(uNF e +Tϑ:N1 0 ~ 2 0 0 m g . k g
1 vmnlRg0
^laNy1 hQ|R-NReQϑ}vl, Onm|^ N0S7h1 . 5 g , R}vl2 . 0 g 0( 2 ) (WSknmTՋ7hnmKm[vGk gQ,
NeUeQzz}vnm, NOcKmϑagNv N'`0
6 . mnl-NAvKm[
S N[ϑvwlxx( S_vQ-N+Tϑ(ϑk:N4 ]Se, ~S5 g ) , nN1 L nBRl-N, Onm-N+Tϑ~:N2 0 0 g . m L - 1 , \O:Nzz}vnm0(u g:gё^\AvR6 m L 2 - YNW]x0ϑ}vlM6RhQPYm0(uzz}vnm zʑhQPYmM6RhQ]\O|Rnm0QnxyS0 . 1 ~ 0 . 3 g Ջ7h( Qnx0 . 1 m g ) N2 5 m L [ϑt-N, (uzz}vnm;3 4 = zʑ;R^0
Km[agN:N: lM g 2 8 5 . 2 n m op5uAm 5 m A IQ1&^[0 . 3 8 n m 0zzlAmϑ1 0 L . m i n - 1 YNpAmϑ1 . 5 L . m i n - 1 qphVؚ^ 4 m m 0ՋmcSϑ2 . 8 L . m i n - 1 0(uhQf~l[ϑ !hckf~v~'`V/f0 ~ 0 . 4 m g . L - 1 0,gl(uNA+Tϑ:N0 . 0 2 ~ 0 . 3 ( m / m ) vmnlRg, _N(uNKm[mRBR-NvA+Tϑ0
7 . mnl-NvKm[;3 7 =
yS2 g Ջ7hnNwiWWQ, (W)n^:N5 5 0 2 5 !vؚ)np-NۏLppSYt, ppS[hQTQtS0KNTReQ1 g &qkxx, (W5up
NRpb_b Nnoqir0QtST\p4lPeQiWWQ, _pOvQn0傔qir gmJmQs, ^ReQϑv1 0 ( v / v ) H 2 S O 4 nm, OvQon, Te(Wzz}vThm-NReQI{ϑvH 2 S O 4 nm0Ջ7h-N+T gC a 0F e yP[, ^Onm-N+T g2 N H 4 C l T0 . 5 A l C l 3 , Nmdr^pb0
(uvKm[agN:N: lM o 3 1 3 . 3 n m zz_4gop5uAm9 m A 0zzlAmϑ1 0 . 0 L . m i n - 1 YNpAmϑ4 . 0 L . m i n - 1 qphVؚ^7 m m 0ՋmcSϑ2 . 8 L . m i n - 1 0(uhQf~l[ϑ0
RhV6es:N9 5 ~ 1 0 0 R S D \N3 . 0 ]\N0 . 0 0 3 0!hckf~v~'`V/f5 ~ 4 0 m g . L - 1 0,gl(uNmnl-NM o ( ;NNkxSpW|ReQ) +TϑKm[0
+Tϑk(W3 : 1 N Ne, (uzzl- YNpkp0q
Nr^pbKm[;3 4 =0v r^pbvQ+TϑXR X'Y SReQN H 4 C l TA l C l 3 egb6Rr^pb 0
8 . mnl-NuϑŔMAvKm[
QnxyS0 . 5 0 g Ջ7hN5 0 m L ZV lYNpQR{-N, R3 m L 1 : 1 H C l nm, 3 n1 : 1 H N O 3 nm0\QR{>eeQ
Nn7h9_Q;1 8 =, >e}YWGrSQYv,
N'}h0>eeQ1 6 0 !R`)n{QmS3 h , SQQtST, 7hmyeQ2 5 m L [ϑt-N, N4l[[0
Km[e@b(uRg~lR+R:NP b 2 1 7 . 0 n m 0N i 2 3 2 . 0 n m 0C o 2 4 0 . 7 n m 0M g 2 8 5 . 2 n m op5uAmP b :N3 . 2 m A , N i 0C o TM g :N3 . 0 m A &^[^GW:N0 . 2 n m 0YNpAmϑR+R:N2 . 0 0 L . m i n - 1 02 . 0 0 L . m i n - 1 01 . 7 5 L . m i n - 1 01 . 7 5 L . m i n - 1 kp0qؚ^P b TM g /f2 2 m m N i TC o /f1 8 m m 0NhQf~l[ϑ0
elvRhV6esP b 0N i TC o :N1 0 0 M g :N9 7 . 5 0R S D R+R:N4 . 0 03 . 8 01 . 9 T2 . 5 !hckf~v~'`VR+R:N0 . 0 5 ~ 5 . 0 0 m g . L
1 00 . 0 6 ~ 4 . 0 0 m g . L
1 00 . 1 2 ~ 5 . 0 0 m g . L - 1 T0 . 0 2 ~ 5 . 0 0 m g . L - 1 0
,gl(uN+TmRBRmnl-NŔ0M00AvRg07hT-NqQX[CQ }+TϑGWNONr^pbAQe(Wؚ)npQN4 5 0 ~ 6 0 0 !|pp, v0Rp=\kp, N,`Q N2 h sSS0O(uppSRBRSOۏ g:girvR㉌Tcؚё^\CQ }vV6es08^(uvppSRBR gSmH N O 3 0SmH 2 S O 4 0K 2 S O 4 0M g ( N O 3 ) 2 I{, SmH N O 3 w'lS\O(u, R g:girvR, SmH 2 S O 4 4xOW g:gir, $\vQ/fZTir0
ؚNO)nppSl(WRgZTir-Nvuϑё^\, $\vQ/ff%cSё^\e, yr+R gHe, FOvQppS ^_( Nm g " h - 1 ) , 'lS ^NoS`'lvSm^0 g:gՋ7hvhb'`(SSf[yr'` gsQ, ^(u g N[v@\P0
ُ{|7hTvWSOr^pb ge^8^%N͑, Yaj6RT, gpSvx0xnvC a C O 3 0nvS i O 2 0nvv WTnw|0@wrvv0}v|T }vI{0O_~b0R(u@b g`Qvr^pbb6RelvS_V, ge (uhQReQl, b(W6RYhQnme=\ϑ9SMՋ7h~b0
fOPNO0xmSTY
NۏL]xSYt, zz}ve(WΘg-N%cS[hQ~ 2 h 6qT(u5 m L 4lm{X R3 m L 1 1 ]xx Rpl~~2 m i n QtST(uSyP[4lly5 0 m L [ϑt-N ReQ/lS6nm\Oʑ>eBR [[ TeZPzz}v0hQf~l[ϑ0
Km[agN:Nop5uAm1 5 m A l2 4 8 . 3 n m IQ1&^[0 . 2 n m YNpSR0 . 3 5 k g . c m - 2 zzlSR0 . 5 k g . c m - 2 0~'`V:N0 . 0 0 ~ 0 . 5 0 m g . L - 1 0R S D :N0 . 1 0 % 0
,gel(uNP V C uN-N/lYNpUSSO-N+TϑKm[ v[krl ,gl gupOe^ؚ0 b'`}Y0͑s'`}Y0{O_ I{yrp0
3 . P E T hSbWT-NvKm[
[Nh7hT, SS4 g nN2 5 0 m L VAmňnvpt-N, ReQ1 0 0 m L 4 YNx, c}YQQ{, (Wl4ltm-NVAm2 h , zsS(u_ n~Ǐn, v^(u\ϑYNxnmmmk#n, Tv^nmT[[1 0 0 m L \O:N7hm0bWTRN1 c m 2 7hTR2 m L 4 YNxnmvkO, (u N[ϑYNxnm(W6 0 ! Nxml3 0 m i n ( Sp[hVR(W9 5 ! Nxml3 0 m i n ) , Sxmlm\O:N7hm;5 1 =0hQ|R T7hN4 YNx zʑ b0
Km[agN:NlS b 2 1 7 . 6 n m op5uAm1 0 m A 0ۏ7hSOy2 5 L 0r^q)n^7 5 ~ 9 0 !, e5 0 s ppS)n^7 0 0 !, e1 2 s SP[S)n^2 1 0 0 !, e4 s QS)n^2 2 0 0 !, e1 s 0Kmϑe_:N\ؚ hQf~l[ϑ0
R S D /f3 . 1 ( n = 1 0 ) , hQf~v~'`V:N0 ~ 8 0 g . L
1 , RhV6es:N9 1 . 7 ~ 9 7 . 7 0
qQX[CQ }P b 0S n 0C d 0Z n Sm^:N1 m g . L
1 e
Nr^pbKm[0Sm^:N3 m g . L
1 e, P b 0S n gckr^pb, Z n 0C d g r^pb0st[ g N[8TD, 7hTYtT^=\_Rg0
4 . ZNp-N_ϑvKm[
yS3 . 0 0 0 g ]S7hTnNwiWW-N, RppS, _pQ=\pS[hQTQN6 5 0 !ؚ)np-N|pp1 . 5 h , ppS[hQ, QtSTSQ R1 0 m L 1 : 1 H C l , baRpiR2 m L ]S, QtSTyeQ2 5 m L Ջ{-N, (u0 . 5 H N O 3 [[;5 2 =0
Km[e@b(ul:NT i 3 6 4 . 5 n m op5uAm2 0 m A &^[^0 . 5 n m 0ۏ7he_:NꁨRmT0wXp)n^ z^Yh1 2 . 5 @b:y0(uhQf~l[ϑ0
h1 2 . 5 Km[agN
ek 1 2 3 4 5 6 7 8 )n^/ ! 9 0 1 1 0 2 0 0 8 0 0 8 0 0 2 8 0 0 2 8 0 0 2 8 0 0 e/ s 5 . 0 4 0 . 0 1 0 . 0 5 . 0 5 . 0 1 . 0 2 . 0 1 . 0 )llAmϑ/ L . m i n eUSMO/ / / / / / L m i n - 1 3 . 0 3 . 0 3 . 0 3 . 0 0 . 0 0 . 0 0 . 0 3 . 0 !hQf~~'`V:N0 ~ 1 m g " L - 1 Km[vR S D :N2 . 3 ( n = 6 ) RhV6es(W9 3 ~ 1 1 7 0
1 2 . 3 . 2 . 3 aj-N_ϑCQ }vKm[
1 . vKm[
QnxyS2 . 0 0 ~ 1 0 . 0 0 g ]Sv u0mpbkxS7hT, \vQqpppSTy͑0RSpp0 . 0 8 ~ 1 . 0 0 g ]S>eeQtiWW-N, (W5up
NpS'YRp( p[THTpp}vr) , leQ2 0 0 m L pog-N, R1 5 m L 1 : 1 H N O 3 05 m L H C l O 4 T(W5up
NRpўr*S, leQ1 0 0 m L [ϑt-N, c0 . 4 g C a C O 3 00 . 4 g B a 00 . 3 3 g A l 2 O 3 00 . 2 5 g Z n O 00 . 0 5 g C o kOϑ ReQmdr^pb~R;5 3 =0(u4l z;R^0
RglF e 2 4 8 . 3 n m zz_4gop5uAm6 m A IQ1&^[0 . 2 n m 0ؚS - 4 7 5 V 0zzlAmϑ5 L . m i n
1 YNpAmϑ1 . 4 L . m i n
1 qphVؚ^( h:\) 5 c m 0Kmϑe_:NSIQ_g0(uhQf~l[ϑ0
elvyr_Sm^:N0 . 1 7 m g . L - 1 NF e 2 O 3 v[] 3 . 6 6 {/gs^GWOP]0 . 0 0 3 1 hQe] 0 . 0 0 4 0 0
[ajWSO
YBg, r^pb%N͑, (WhmT7hT-NReQmdr^pb~R, W,g
NmdqQX[CQ }vq_T0KmՋN((u1 ~ 4 H N O 3 e
Nq_TKm[~g, S
NOQskxxlm0
2 . Tbaj-NvKm[
S4 . 0 g 7hTN'lSݔiWW-N, RppS g:gir, 6qTleQؚ)np-NN5 0 0 !|ppO7hT-Nvx[hQ'lS, QtST, ReQ1 0 m L s4l, Rpn㉋k#n;4 2 =0~Q!kQtSTly5 0 m L [ϑt-N, (u4l zʑ;R^, Gd S
Rg~l:N F e 2 4 8 . 3 n m , C a 4 2 2 . 7 n m , N a 5 8 8 . 9 n m 0zz_4gop5uAm:N1 0 m A IQ1&^[:N0 . 3 3 n m zzlSR1 . 8 k g . c m
2 , Amϑ1 4 L . m i n
1 YNpSR0 . 5 k g . c m
2 , YNpAmϑKm[F e TN a :N3 . 5 L m i n
1 0Km[C a :N4 L m i n
1 0(uhQReQl[ϑ0RgV/fF e 0 . 0 ~ 0 . 1 m g . L
1 , C a 0 . 0 ~ 0 . 3 m g . L
1 TN a 0 . 0 ~ 0 . 3 m g . L
1 0
Ջ7h-N_KmCQ }+TϑǏؚe, ^ zʑTQۏLKm[0
3 . sN-N_ϑCQ }vKm[
S5 0 m L sNmleQv_:N1 2 c m vW{Qv-N, Gd S, s^nNp{-N (W)n^7 0 ! Npr^06Rbv_1 2 c m 0S0 . 2 c m vr^Gr0 cVRljRS@b 7hT, KNT(u5 H C l T4lmQ0pr^0(unmSlbr^ppSlYt7hT;5 4 =0
( 1 ) nmSl S2 g r^7hTnN5 0 m L Qlt-N, ReQ4 ~ 5 |sts, QR5 m L SmH N O 3 (W5up
NNO)nmS0_Gr[hQRN ghrpQQe, ReQ1 . 5 m L H C l O 4 , ~~Rpm, v0R g}vpQQN7hmerf:Nbk0RpvSYYOvH C l O 4 7hmiR1 m L ]SeS N, QtSTly[[5 0 m L [ϑt-N0
( 2 ) r^ppSl (un~\2 g 7hTSOOnN5 0 m L iWW-N, NO)nppS1 5 m i n , QN5 5 0 !ؚ)np-NppS v7hTHTpp}vr:Nbk0SQQtST(u2 0 m L 1 : 1 H C l nppSir, [[5 0 m L 0
(ukp0qSP[8T6eIQ1lKm[, Km[agNSSvQNvsQe.s0
,gl(uNKm[sN-NK 0C a 0M g 0C u 0M n 0Z n I{CQ }vKm[ qQX[CQ }
Nr^pbKm[0
Km[e laNy:NnmS7hTe)n^NO, N HQ(uH N O 3 R g:g(TQRH C l O 4 0r^ppSe(un~SOO7hT, e2bk7hTNzzlcwkp, Sb_b NyQSR2bk7hTfl0
4 kp0qlKm["lSNHajPSBR1dm-Nє[ 5 5 ]
ϑS N[SOyv"lSNHajm ReQ0Rň gdbTVAmQQ{v NSt-N db4lGS)nReQ N[ϑ~TBRkx2 dbS^ NkeT \PbkRp0db v^TS^m-NReQ N[SOyvxmSBR8 8 % 2ux Q/cadb KNTYnRyby_Ry 6eƖ NB\+Tєv4lv Km[є+Tϑ0
NhV]\OagN:Nop5uAm1 0 m A lR h 3 4 3 . 5 n m IQ1&^0 . 4 n m kp0qؚ^7 . 5 m m YNpAmϑ2 . 0 L . m i n - 1 zzlAmϑ9 . 5 L . m i n - 1 0hQf~l[ϑ ~'`V0 . 0 0 ~ 8 . 0 0 m g . L - 1 0RhV6es:N1 0 0 . 5 % ~ 1 0 1 . 5 % R S D :N1 . 6 % ~ 1 . 8 % 0,gelS(uNxvz~T- xmSl1d"lSNHajPSBRR h C l P P h 3 3 v]zagN0
1 2 . 3 . 2 . 4 me-N_ϑCQ }vKm[
1 . vKm[
QnxyS0 . 2 0 0 0 g Ջ7hnNQXeiWW-N, N\ϑ4lmn, ReQ5 m L H F 01 m L H C l O 4 , (Wwhg
NRpR, }vpQ=\0R3 m L H C l ( 1 + 1 ) , )npnv{|, QtST, yeQ2 5 0 m L [ϑt-N[[09hncF e 2 O 3 +TϑRSRnm0R2 5 m L kr{-N, ReQ2 . 5 m L 1 0 g . L
1 vbOW@x, \nm-NF e 3 + ؏SbF e 2 + 0QReQ2 . 5 m L 5 g . L
1 v1 , 1 0 N.lBg( p h e n ) nmT1 . 0 m L H C l O 4 ( 1 + 3 ) Gd S, (u1 . 0 m o l . L
1 N a O H nmp H (W2 . 0 ~ 3 . 0 KN, >en3 0 m i n Tb_byP[TirF e [ p h e n ] 3 2 + [ C l O 4 - ] 2 0ReQSBR]xW2 . 5 m L , /cGd3 m i n , RB\T(ukp0qSP[8T6eIQ1lKm[ g:gv-Nv;5 6 =0
Km[agN:NlF e 2 4 8 . 3 n m op5uAm4 . 5 m A IQ1&^[0 . 2 n m 0qphVؚ^8 . 0 m m YNpAmϑ2 . 0 L . m i n
1 zzlAmϑ5 . 6 L . m i n
1 0
elvhQP:N1 . 1 n g . m L
1 R S D /f1 . 5 2 ~ 3 . 5 7 ( n = 6 ) RhV6es:N9 8 . 5 ~ 1 0 6 0!hckf~v~'`V:N0 ~ 4 . 0 g . m L
1 0
[NKm[3 m g . L
1 F e 2 O 3 , Bl8TIQ^]
NǏ 5 e0qQX[yP[ gؚAQϑ:N: C a 2 + 0M g 2 + 0S i 4 + 0A l 3 + 0F - 0C l - /f5 m g M n 2 + 0C o 2 + 0N i 2 + 0C u 2 + 0P b 2 + 0Z n 2 + 0S O 4 2 - 0N O 3 - 0C 2 O 4 2 - 0C O 3 2 - /f1 m g C r 3 + 0V 5 + 0M o 2 + 0C d 2 + /f0 . 5 m g 0
2 . "lSirS ulKm[^l
yS2 . 0 0 . 0 1 g 7hTnN2 5 0 m L pog-N, R5 0
P( m / m ) N7hTϑv0 . 0 7 m o l . L
1 vvxnm, /ca1 m i n , KmϑmTmvx^, (u1 m o l . L
1 H C l p H :N1 . 0 ~ 1 . 5 , dbmTm1 h , Ybk1 h , ۏLVmRy06qTǏnhV( T[_0 . 4 5 m ) Ǐn1 0 0 m L [ϑt-N, [[T8TS勶nm2 0 m L y2 5 m L [ϑt-N, R1 . 2 5 m L 5 ( v / v ) H C l T2 . 5 m L 0 . 5 K 2 C r 2 O 7 nm, (u4l zʑ;R^0
7hmۏeQAmRl\N, Am :N2 . 0 m L . m i n
1 }Am( 5 H C l ) Am 1 6 m L . m i n
1 N0 . 1 2 5 K B H 4 nm(W~mT, (Wx'`agN N؏Sb^l, 1u1 5 0 m L . m i n
1 A r l&^eQwSP[ShVKm[;5 7 =0(uhQf~l[ϑ0
elvhQP:N0 . 0 5 8 g . L - 1 R S D ( n = 1 0 ) /f3 . 1 RhV6es:N9 3 . 5 ~ 1 0 8 . 0 0,glKm[v/fme-NSn'`^l _N(uNme-NuϑA s 0S b 0S e I{CQ }Km[0
3 . lo-NŔvKm[
\lo>eeQ]R`͑vyϑt-N, _ y͑TN1 0 5 ! NRppr^, BlQ%cSirv~vR+Tϑ0\pr^Tvlox~, v^S1 0 0 m g nN5 0 m L pog-N, (W4 0 0 !ؚ)np-N|pp1 h , dS g:gir SQQtSTReQ4 0 m L ( 1 + 1 ) H N O 3 , Rpn, Sm)iR1 0 m L ]Se, S NQtS0ly1 0 0 m L [ϑt-N(u4l[[0Y gk#nSǏn0
RgagN:N: lP b 2 8 3 . 3 n m IQ1&^[0 . 7 n m 0YNpSR1 . 5 k g . c m - 2 YNpAmϑ( pe) 3 0 zzlSR2 . 0 k g . c m
2 zzlAmϑ( pe) 6 0 0qphVؚ^( h:\) 7 0lopcb̀of0(uhQReQl[ϑ0
qQX[CQ }F e 1 0 0 0 m g . L
1 0T i 5 0 m g . L
1 0Z n 1 5 0 0 m g . L
1 0S i 9 0 m g . L
1 0C a 2 0 0 m g . L
1 0M g 2 0 0 m g . L
1 0C r 5 0 m g . L
1 0A l 1 0 0 0 m g . L
1 0 C u 2 0 0 m g . L
1 e[5 0 m g . L
1 P b vKm[er^pb0
RgV:N0 . 5 ~ 3 0 RhV6es:N9 7 . 5 ~ 1 0 3 0
4 . ZT~g-N vKm[
\|xTv7hTǏ8 0 v[{, yS~0 . 5 g nN5 0 m L %b_t-N, ReQ2 0 m L 9 5 YN, 4ltm_pOKNn㉌[hQ, ly5 0 m L [ϑt-N, (uYN zʑ;R^;5 9 =0
Km[evl:NZ n 2 1 3 . 9 n m op5uAm1 . 5 m A IQ1&^[0 . 2 n m 0zzlSR0 . 1 5 M p a zzlAmϑ4 . 5 L . m i n - 1 YNpAmϑ0 . 4 L . m i n - 1 0qp4Yؚ^4 m m 0yRe1 . 0 s 0ՋmcGSϑ5 m L . m i n - 1 0(uhQf~l[ϑ0
elvyr_Sm^0 . 0 0 7 7 m g . L - 1 R S D :N1 . 1 ~ 4 . 1 ( n = 1 0 ) RhV6es:N1 0 0 . 9 ~ 1 0 2 . 9 0!hQf~~'`V:N0 ~ 1 . 0 m g . L - 1 0
qRk0ՋmcGSϑ_{N~0
1 2 . 3 . 2 . 5 ZoNTSvQSe-N_ϑCQ }vKm[
1 ZYCQ-NvvcKm[
QnxyS1 . 0 0 0 0 g 7hT, (uYN- 4lmTmn, KNTly[[N2 5 m L [ϑt-N;6 0 =0hmN(uYN- 4lmTm zʑM6R0
Km[lK 7 6 6 . 5 n m , N a 5 8 9 . 0 n m op5uAm:N1 0 m A &^[^K /f2 . 6 n m , N a /f0 . 4 n m 0zzlSR/f0 . 1 6 M p a YNpSR/f0 . 0 1 5 M P a 0(uhQf~l[ϑ0
,gl(uNyP[+Tϑ'YN1 m g . k g
1 v7hT, S_7hT-NyP[+TϑNON0 . 5 m g . k g
1 e, X'YS7hϑ O7hm|^X'Y, Vdk[Ǒ(uppSlYt7hT0
2 . [N2ux-N_ϑё^\Bg(Km[
ySmTGW Sv7hT2 5 . 0 g nN1 5 0 m L N҉pt-N, ReQ5 0 . 0 m L 5 % ( v / v ) H N O 3 nm, >e(WxRdbhV
Ndb2 5 m i n , 6qT wzzǏn07hT-NvM n 0C o 0C r 0F e 0N i I{ё^\Bg(Sۏnm;6 1 =0
Km[agN:N: lM n 2 7 9 . 5 n m C o 2 4 0 . 7 n m F e 2 4 8 . 3 n m N i 2 3 2 . 0 n m C r 3 5 7 . 9 n m 0IQ1&^[C r :N0 . 5 n m vQYOCQ }:N0 . 2 n m 0YNpAmϑM n :N2 . 0 L . m i n
1 C r :N2 . 8 L . m i n
1 vQYOCQ }:N2 . 2 L . m i n - 1 zzlAmϑGW:N9 . 5 L . m i n
1 0qphVؚ^C r :N9 m m vQYOCQ }:N7 m m 0(uhQf~l[ϑ0
TCQ }vhQPS0 . 1 m g . k g
1 0R S D ( n = 6 ) R+R:NM n 2 . 5 C o 1 . 8 F e 5 . 3 N i 2 . 7 C r 8 . 8 0RhV6esR+R:NM n 1 0 5 C o 1 0 9 F e 9 5 N i 9 2 C r 9 4 0
Ջ7h-Nё^\Bg(+Tϑ_NO, CQ }KNN
Nr^pb0,glke:gppSl{O0_ 0Qnx
xnmN7hTvkOq_TSHes, S_mTk< 0 . 5 e, VSO+Tϑؚ, dbVmTk> 1 e, Ss3z[, FOmTkǏ1 0 e, _KmCQ }Sm^*YNO, NQnx[ϑ0SY [N2ux}
NnN4l, FO8Tn'`}Y, N4lm S, fNS0
3 . ZoRGr-N_ϑvKm[
yS1 . 0 0 0 0 g ~ 1 . 2 0 0 0 g RGrnN1 0 0 m L %b_t-N, ReQ5 m L SmH 2 S O 4 , (W)n^-Nv5upg
NRp Ջ7hpSv^QQSmH 2 S O 4 v}vp0\mSiň(Wpt
N 6qTR N[ϑv3 0 H 2 O 2 0RRm{-N0;m^X, OH 2 O 2 Nky1 nv ^AmeQ%b_t-N, ~~Rpv^nRH 2 O 2 ~2 0 ~ 2 5 m L , Ջ7h[hQR, nmSn, ~~nqlnmĞhrm1Y, dkeH 2 O 2 [hQdS;6 2 =0S NQtST(u4l[[5 0 m L 0傟S7hT/fmIQRGr, VvQ-N+TT i O 2 , YtTv7hm:NĞr0
Km[agN:N: lS b 2 1 7 . 6 n m , zz_4gop5uAm1 0 m A , IQ1&^[0 . 3 8 n m 0zzlAmϑ/f8 L . m i n
1 YNpAmϑ/f2 . 5 L . m i n
1 qphVؚ^3 m m 0(uhQf~l[ϑ0RhV6es9 6 . 5 ~ 1 0 1 0
,glǑ(umSinlYt7hT, wewR, (uNRGr-N_ϑvKm[0
^laNy:N( 1 ) S b /f Nyf4l㉄vCQ }, nmOc N[vx^, &TROQslm07hmNhmvx^9SM0( 2 ) H 2 S O 4 TH C l x^XR, S b v8TIQ^X'Y H N O 3 (W0 ~ 3 . 5 Q, 8TIQ^3z[0H N O 3 > 3 . 5 e, S b 8TIQ^
z gXR0
4 . ZoRGr-NN'lSvKm[
QnxySRGr~1 . 0 0 0 0 g nN1 0 0 m L N҉pt-N, ReQ7 . 5 m L SmH 2 S O 4 T5 m L SmH N O 3 , RpՋ7hSўTS N, QtSTReQ1 m L H C l O 4 , v^RpՋ7h[hQn, 6qTƉ&^r z^mEmQR0 . 5 ~ 1 m L H C l O 4 , ~~Rpnmerf0Sm)iR2 m L ]S0S NQtST[ϑly0R5 0 m L [ϑt-N, ReQ1 0 m L 5 g . L - 1 NN a N a C l nm, (u4l z;R^;6 3 =0
ReQN a C l nmKQ
gNؚ)nkp0q-NT i v5uyr^pb, 7hT-NvؚZirWSOSqQX[CQ }[Km[eq_T0KmՋ+Tϑ:N0 . 5 vT i O 2 , R S D ( n = 6 ) :N0 . 9 4 RhV6ess^GW:N1 0 1 . 2 0
Km[el:NT i 3 6 5 . 4 n m , zz_4gop5uAm1 0 m A IQ1&^[0 . 2 n m 0\C 2 H 2 TN 2 O vSRNAmϑ gsOMOn qphVؚ^:N9 m m 0ՋmcSϑ7 . 5 m L . m i n
1 0yRe1 s 0(uhQf~l[ϑ0
7hT+TϑNOe, Km[~g]'Y, ^S_XRS7hϑ0Km[eH C l eq_T, H 2 S O 4 gf>f r^pb Ee(Whm-NReQϑH 2 S O 4 N9SM7hm~b0
1 2 . 4 PSBR0mRBRT|~S]NTvRg
1 2 . 4 . 1 7hTMRYti;1 1 , 1 3 , 6 4 6 5 =
PSBR0mRBR0nBR Oy]N NBR 0Y|~S]NT_NNmRBRvb__Q
gRN uN, PSBR,g_N{ Ny|~S]NT0
wlS][E
N/fNPSBR:N-N_v N*NLN nc~ 9 0 N
NvwlSf[S^/fǏPSBReg[sv;6 4 =0PSBRvSf[~bSb: ;NPSBR0RPSBRT}SO NR0 c(uSR:NPSS0PS͑te0R"l|6R0s'lYNp02ugkS0ppZTI{Yy{|WvPSBR0 c}SOSR:N: 'lSݔ0Ex0;m'`p0;m'`AI{Q{| N'lSݔTExPSBRE\Y0;m'`APSBR;N/fZppPSBR g͑v/fZ i e g l e r - N a t t a WPSBR vQ8^(u}SO/f~yrkYtvM g C l 2 0
mRBR(W uNǏ z-N\O:NRBR w0RcؚNT6es R'Y uN w 9eUNT'` Q\YPv\O(u0YSBR[MNOPSSňnv"llT&qpNϑ cؚlSsT{l6esGW go}YvHeg FOSBRvReQϑc6Rϑ;6 6 =0+TϑǏ N[P^e "llT&qpNϑGW g
NGS0wlNTTZTir-NReQvb'lBR0BR0IQlBR0XQXBR0mnBRI{ gvS_͑v\O(u0
PSBR0mRBRT|~S]NT-N_ϑCQ }Rg N/fRg,gV gbR Q:NvQalgCQ } YS]Se-N_ϑCQ }vRg_N^\NalgCQ }vRg0nce.s;6 4 =N~ [ё^\PSBR g[f-Nkv;m'`PSё^\:NF e 0R u 0O s 0C o 0R h 0I r 0N i 0P d 0P t 0C u 0A g 0A u I{0h1 2 . 6 :yQN NNPSS^-N_wPSBR-Nkvkir0
h1 2 . 6 NNPSBRvkir
PSBR S ^ k ir N i , P t , P d , C u R"l 1"l S , S e , T e , P , A s , S b , B i , Z n , H g , P b ,
N H 3 , M e 2 S , !TvU, O 2 N i , P t , P d , C u 'lS v'lSir 7xSir Sir YNp H 2 S Exxݔ ExxA
;m'`}v W p{|R pWS _gS ZT UIU g:gx 4l ͑ё^\ C r 2 O 3 - A l 2 O 3 p{|gS H 2 O P t - A l 2 O 3 , P d }ll͑te kxvSTir V 2 O 5 , V 2 O 3 'lS 7xSir A g 'lS C H 4 , C 2 H 6 S i O 2 - A l 2 O 3 S !TvU UIU H 2 O ͑ё^\STir
x'` g:gir C o R"l N H 3 , S , T e , S e , P vSTir F e , C o F i s h e r Tb S , ! C o WTbS^ S F e Tb(l S vSTir O vSTir C u , C l 2 , P I{ P d 2uxR 7xvSTir P t - A l 2 O 3 }lf>\lQS F e , C r , C u I{
PSBR-NvgNё^\ YP d 0A g /f(WPSBR6RYǏ z-N xm
n(WWSO
Nv gvS(uxxmS Neg ǏnTRgnmsSS
N bWSOhQ萶n0
(uǏvPSBRhb gyp HQۏLppYt06RY7hTe^HQOvQGWS;1 3 = lx(7hTSǑ(uxS0xx0|S0ccxI{Kbk o(bJSo(7hT RǑ(uRx0cT0~xNSGW(S 7hTGW SNTQZPۏ NekvYt0dk{|7hTv6RY g͑v/fqbn SǑ(uxn0xn0vn0 g:gnBRn ge (uؚSn b PR_lm0
Rgُ{|7hTeQ0RWSOvq_TTqQX[CQ }vr^pb yr+R/fY7hT-N+T gS i r^pb͑ S(uhQReQlKm[bRr^pbb6RBR0YKm[C a 0M g eReQL a 0S r \O:Nʑ>eBRegmdA l vq_T b(WM6RhQ|Re !jbՋ7hnm-Nvr^pbCQ }+Tϑ ReQϑvr^pbCQ }N9SMՋ7h~b0
1 2 . 4 . 2 7hTRg
1 2 . 4 . 2 . 1 PSBR-N_ϑCQ }vKm[
1 . vKm[
\PSBR7hTx~, (W1 2 0 ! Nr^q4 h 0yS0 . 1 0 0 0 g 7hTnN5 0 m L pog-N, ReQ2 m L H 3 P O 4 + H 2 S O 4 mx( 2 + 1 ) , Rpn, QtST(u1 H N O 3 ly5 0 m L [ϑt-N[[, Q(u1 H N O 3 zʑ5
PT\O:NKmՋnm0
Km[agN:NlA g 3 2 8 . 1 n m zz_4gop5uAm4 m A IQ1&^[1 n m 0+qkp0q0(uhQf~l[ϑ0
elvyr_Sm^:N0 . 0 5 m g . L - 1 !hQf~v~'`V0 ~ 1 . 5 m g . L
1 0,gl(uN'lSݔ}SOPSBR-NA g 0P d +TϑvKm[0
7hTWSO;N:N'lSݔ Ջm-NA l +Tϑ~:N2 0 0 m g . L
1 , :Nmd'YϑA l vr^pb, (WhQnm-N_NOA l Oc(W2 0 0 m g . L
1 0(ukxxmxYtؚ)np~v'lSݔ}SOPSBR, Heg}Y;6 7 =0FOmx[A g g_1_r^pb, hQnmTzz}vnm-NGW^ReQ Tϑmx, NNՋm9SM0
2 . ͑tePSBR-NuϑBg(A ŔvKm[
QnxyS0 . 3 5 ~ 0 . 4 0 g 7hTnNZV lYNppog-N, R3 m L SmH C l 01 m L 4lS3 ~ 5 nSmH N O 3 , \SR[9_[T >eeQ1 8 0 1 0 !p{QRp4 h Nm7hT, QtSTSQ, yeQ5 0 m L [ϑt-N0Km[C a 0M g e^ReQ4 m L 1 0 m g . m L - 1 K C l nm, (u4l zʑ;R^;6 8 =0
(uhQf~l[ϑ0Km[agNYh1 2 . 7 @b:y0
h1 2 . 7 Km[agN
CQ } l
/ n m op5uAm/ m A zzlSR/ k g . c m - 2 YNpSR/ k g . c m - 2 N 2 O SR
/ k g . c m - 2 qp4Yؚ/ c m r / NhVpe ̀of
cbd C a 4 2 2 . 7 7 . 5 0 . 3 5 3 . 0 2 2 M g 2 8 5 . 2 7 . 5 0 . 3 5 3 . 0 2 2 Z n 2 1 3 . 8 7 . 5 1 . 6 0 . 2 0 4 2 lop P b 2 1 7 . 0 7 . 5 1 . 6 0 . 2 0 2 2 lop Km[C a 0M g (u'lSN.lYNpkp0q, Nb6Rnm-NA l vr^pb, ReQK C l nmSb6Rdkkp0qagN NC a 0M g vyP[r^pb0S_CQ }+Tϑ:N0 . 0 0 0 1 ~ 0 . 0 9 e, s^LKm[vAQv[OP]: M g 0C a TZ n /f1 5 0P b /f3 0 0
,gl؏(uN͑tePSBR( SbPSBR}SOTؚ~'lSݔ) -NuϑBg(P t 0S n 0S i 0F e 0N a 0C u vKm[0
sSOǑ(u N'lSN.lYNpkp0q, A l vr^pb_NN[hQb6R0Vdk, C a 0M g 0Z n 0P b hQnm-NReQϑv1 0 m g . m L - 1 A l N(nm, N9SM7hmv~b0C a 0M g (uUS NCQ }hQ|RZ n 0P b (umThQnmsSS0
3 . PSSPSBR-Nv͑ё^\+TϑvKm[
yS7hT0 . 2 g nNmSPQ, R1 0 m L 1 : 1 H C l T0 . 5 m L H F , v}Y
Nvv^>eeQ2r, e'}KNT>eeQ_lpQm;6 9 =0\m}Yv7hTly0R2 5 m L QXe[ϑt-N, (u4l zʑ;R^, Te\Ozz}vnm0dk7hmSvcKm[C u , zʑ5 0
PTKm[F e TN i 0
V ^\Nؚ)nCQ }, (Wzzl- YNpkp0qll N, SP[SHesNO, Ee(uwXpSP[SlKm[V NhQf~l[ϑ0
,gl(uNPSSs^aPSBR-N͑ё^\+TϑKm[0k(umx _SmlYt7hTew,
NalgsX0
Km[e (uvRgl:NF e 2 4 8 . 3 n m 0N i 2 3 2 . 0 n m 0C u 3 2 4 . 8 n m 0V 3 1 8 . 4 n m 0zz_4gop5uAmR+R:N3 0 02 5 01 5 T4 0 m A 0IQ1&^[F e 0N i :N0 . 2 n m , C u 0V :N0 . 7 n m 0
F e 0N i 0C u (ukp0qSP[8T6elKm[, zzlAmϑR+R:N7 . 9 08 . 6 T8 . 6 L . m i n
1 YNpAmϑR+R:N1 . 0 00 . 9 T1 . 0 L . m i n
1 0V (uwXplKm[, vQ)n^ z^:N: r^q)n^1 2 0 !, Oce3 0 s ppS)n^1 4 0 0 !, Oce1 0 s SP[S)n^2 6 5 0 !, Oce5 s 0
^laNy( 1 ) Nňn
NǑegv7hTN5 5 0 !)n^ Np2 h dp( 2 ) 傈me
NRH F , 7hTn
N[hQ, ~gOPNO0
4 . 'lSvKm[
\PSBR7hTHQ(W5 5 0 !vؚ)np-N|pp1 ~ 4 h dp, KNT(uH F - H 2 S O 4 R7hT, S i ubS i F 4 %cSQS;6 8 =0wQSOd\O:N: QnxyS0 . 2 g ]S7hT( Q0 . 0 0 0 2 g ) Nv-N, (u\4lmn, R4 m L 1 : 1 H 2 S O 4 T2 0 m L H F , GdRT(W5up
NRpS0 _YQQH 2 S O 4 }vpQR, QtSTR1 0 m L H F , ~~QQH 2 S O 4 }vp:Nbk0ReQ2 ~ 3 m L 4lS
YS2 !k0R1 0 m L 1 : 1 H C l , (W5up
N_p, Onm[hQf, ly1 0 0 m L [ϑt-N, [[0
Km[agN:N: RglN a 5 8 9 . 5 n m zz_4gop5uAm3 m A IQ1&^[0 . 2 n m 0zzlAmϑ7 . 0 L . m i n
1 YNpAmϑ1 . 7 L . m i n
1 qp4Yؚ^1 0 m m 0(uhQf~l[ϑ0$N!ks^LKm[vAQ]
N'YN$Ns^GWeeQ1h3 0 g , [hQxml(WnmQ, Rv(W3 8 0 . 5 !p{Q>e4 )Y0SQTnr^, (u4lmя-N'`, Jd _N3 5 !]Spr^, [IQOX[0
7 . kp0qSP[SlKm[
yS]x~v7hT0 . 1 0 0 0 g NSR[9_vZV lYNppog-N, R3 m L s4l01 m L H F ( 7hTfn, S
NRH F T|xxnm) 01 m L SyP[4l0\SR[9_>eeQ1 8 0 !vp{-NR`)n3 ~ 4 h , QtSTSb _SR[9_, ReQqT|xx4lnm~1 0 m L , leQ5 0 m L [ϑt-N, [[0SՋm5 ~ 2 0 m L nN2 5 m L [ϑt-N, ReQ2 . 5 m L 1 5 C u S O 4 nm, [[;6 8 =0
Km[agN/fl:NP t 2 6 5 . 9 n m zz_4gop5uAm7 . 5 m A IQ1&^[0 . 4 n m 0zzlSR1 5 2 k p a YNpSR1 4 . 7 k p a qp4Yؚ^1 . 5 c m 0lopcb̀of0(uhQf~l[ϑ0s^LKm[vv[OP]
N'YN4 0
Nkxxܔ:Nʑ>eBRb6Rr^pb0,gl(uNRP[[{PSBR0͑tePSBR0(lnm0/lxnm-N+TϑKm[0
8 . SwXplKm[uϑT
yS0 . 5 ~ 1 g NExݔ:NWSOv7hT, nNZV lYNppog-N ReQ2 0 m L 8 m o l . L
1 vH C l 05 m L H C l O 4 T5 m L H F , (W5up
NNO)nRp( < 1 6 0 !) QsH C l O 4 }vp0[N'lSݔ:NWSOv7hT, nN5 0 m L stpog-N, ReQ2 0 m L 8 m o l . L
1 vH C l T5 m L H C l O 4 , Rp7hThQ萶n0S NpogQtST, nR5 m L H 2 O 2 , Q_pOǏϑvH 2 O 2 R0QtSTnmly6 0 m L oe-Nv^(u8 m o l . L - 1 H C l mmpe!k, OnmSOy(W2 0 ~ 3 0 m L KN, ReQ1 m L 0 . 2 SASNpWNkxNYNNp( D D O ) Nnnm 1 m L 5 0 /lSN!v8 m o l . L - 1 H C l nm, Gd STN5 0 !4ltm-NR`)n2 0 m i n 0SQoeQtSTR2 m L N/l2up, /caS1 m i n , hQnm_NN T7hekS, RB\TKmՋ N/l2upnm;7 2 =0
Rgl:NP t 2 6 5 . 9 n m , P d 2 4 4 . 8 n m 0ۏ7hSOy:N5 0 L 0wXp)n^ z^:N: r^q)n^1 5 0 !, Oce3 0 s ppS)n^7 5 0 !, Oce2 0 s SP[S)n^2 6 5 0 !, P t Oce5 s , P d Oce3 s 0lopcb̀of0(uhQf~l[ϑ0
~ N!kST vQSHesS9 5 0hQPP t :N0 . 1 m g . k g
1 , P d :N0 . 5 m g . k g
1 0R S D n = 8 ) P t < 4 TP d < 3 0RhV6es:N9 8 ~ 1 0 4 0
,gl(uNR"lPSBR0͑tePSBR0PSSPSBR-NuϑTvKm[0~ST, qQX[CQ }
Nr^pb0
Km[elav/f( 1 ) Sex^_{(W8 m o l . L - 1 H C l N
N, MbOS[hQ( 2 ) S)n^, P t (W[)n NsSS, P d [)n NS^ba, (W5 0 !4ltm-N1 0 m i n S^sS[b( 3 ) H C l O 4 [Km[eq_T, H N O 3 g%N͑ r^pb0
9 'lSN.lYNpkp0qSP[SlKm[N'lSEx
QnxyS0 . 0 4 ~ 0 . 5 g 7hTNiWW-N, Rpene4lYNmnՋ7h, 6qT(WvQ
Nv4 . 0 ~ 5 . 0 g N a O H , v
NiWWTnN6 0 0 ! NRp1 5 m i n q7hT0SQQtSTReQ1 0 m L SyP[4l, RpxmSqir leQZV lYNppogQ, ReQ2 0 m L 1 : 1 H C l ( bH N O 3 ) xS, _pTleQ1 0 0 m L [ϑt-N, (u4l zʑ;R^;6 8 =0
Km[agN/fl:NS i 2 5 1 . 6 n m zz_4gop5uAm1 5 m A IQ1&^[0 . 2 n m 0N 2 O Amϑ9 . 5 L . m i n
1 C 2 H 2 Amϑ7 . 6 L . m i n
1 0(uhQf~l[ϑ0$N!ks^LKm[vAQ]
N'YNs^GWeeQYWY-N, e'}v=^v^ceQcl{, Te6RYՋBRzz}v0\_lpΘ _ g'Y0 cYekm z^m;7 5 =: z^1 , Rs8 0 , SR8 0 , m1 0 m i n z^2 , Rs1 0 0 SR8 0 m2 0 m i n z^3 , Rs1 0 0 SR1 0 0 m2 0 m i n 0mTleQ1 0 0 m L [ϑt-N, (u4l zʑ;R^, x^Oc(W5 ~ 0 0
(ukp0qSP[8T6elKm[A, Km[agNSvQNe.s, NhQf~l[ϑ0
Km[AvR S D GW\N2 . 9 0RhV6esGW:N9 8 ~ 1 0 1 0,glKm[~gNr^lppS0SRn7hv~g;TT, FO,gl_ {O0
^lav/f( 1 ) s4l[nPP%N͑,
N[(uegm7hT( 2 ) [*gw7hT, HQQYekm z^q`7hT, SՋ(u_ m z^0
3 . AvKm[
SvS_N+TM g ~1 g v7hTnN3 0 m L iWW-N( Qnx0 . 0 1 m g ) 0\ N _[ϑn~[SjR _, wSbW%r_kp, z>e(WiWW-N, \Ջ7hvOO;3 4 =0(W5up
NRpiWW7hTQp, pq_kp, q=\Sqir06qTly8 0 0 2 0 !vؚ)np-NppS2 0 m i n , SQiWWTQ[)n, (u\ϑ4lmnppR, ReQ2 m L 1 : 1 H C l nppR, KNTly1 0 0 m L [ϑt-N, ReQ1 0 m L 3 0 g . L
1 v]xx6nm, [[0
Km[agN:N: lM g 2 8 5 . 2 n m , op5uAm1 0 m A IQ1&^[0 . 7 n m 0zzlAmϑ2 5 L . m i n
1 , YNpAmϑ2 . 5 L . m i n
1 , qp4Yl3 0 ^0yRe2 s , Sm^ve_0(uhQf~l[ϑ0
!hckf~v~'`V/f5 . 0 ~ 2 5 . 0 m g . L - 1 0
(Wĉ[vagN N, Ջ7h-NqQX[CQ }C a 0B a 0Z n 0S 0P [Km[GWer^pb0,gl(uNM g +Tϑ:N1 ~ 1 0 vwlmRBRRg0
4 . mnlmRBR-NvKm[
yS0 . 2 0 0 g 7hT, (u1 0 m L e4lYNnv^ly0R5 0 m L [ϑt-N0(u1 : 1 vV"lKTU- 2uW_NW2un( M I B K ) mTnm zʑ;R^0hQ]\Onm_N(uV"lKTU- M I B K n zʑM6R;7 6 =0
Km[e (uvRgl:NM o 3 1 3 . 3 n m zz_4gop5uAm2 0 m A IQ1&^[0 . 7 n m 0\N 2 O TC 2 H 2 vSRTAmϑ0R gsOMOn0lopcb̀of0(uhQf~l[ϑ07hT-NM o +Tϑ(W3 . 0 ~ 8 . 0 KNe, $N!ks^LKm[eeQmS{Q, R\ϑ4lmn, QR2 m L SmH N O 3 , mS{S
Nc N\stoe0\mShV)n^1 5 0 !, ǏJS\e1\W,gmS[b0Rpv=\N O 2 , Onmяr^, R1 0 m L SyP[4ln, QtSTleQ5 0 m L [ϑtQ, v^9TmstoeQX4lsN[ϑtQ, (u4l zʑ;R^0hmNzz}vnm_N c T7hekmST[[;7 8 =0
Km[agN:N: lF e 2 4 8 . 3 n m , zz_4gop5uAm4 m A IQ1&^[0 . 2 n m 0zzlAmϑ5 . 5 L . m i n
1 YNpAmϑ1 . 2 L . m i n
1 qphVؚ^ 6 m m 0(uhQf~l[ϑ0!hQf~v~'`V:N0 ~ 1 0 m g . L - 1 0
^la/f( 1 ) 7hT (W1 0 5 !)n^ Npp4 h , QtSTr^qOX[0( 2 ) S7hϑYe, S(uhQReQlKm[, Nmd7hT|^vq_T0( 3 ) (uH N O 3 [hQmS7hT, MQSO(uH C l O 4 0
3 . mSOe-Nܔ 0vKm[
ySՋ7h1 . 0 0 0 ~ 2 . 0 0 0 g , nN2 5 0 m L Qlpt-N, ReQSmkxx1 0 m L , RpmS g:gir[hQmT, S NQtS, yeQ1 0 0 m L [ϑt-N, (u4l zʑ;R^0RS N[ϑv TSOyv勶nm0R4 *N5 0 m L [ϑt-N, chQReQlvStM6Rnm0NhQReQl[ϑ;7 9 =0TCQ }Km[agNYh1 2 . 8 @b:y0
h1 2 . 8 Km[agN
CQ } Rg~/ n m op5uAm/ m A YNpAmϑ/ L . m i n - 1 zzlAmϑ/ L . m i n - 1 8T6eؚ^/ m m Km[V/ g . m L - 1 R S D n = 1 0 / RhV6es
/ C u 3 2 4 . 8 8 1 . 2 6 ~ 7 2 2 ~ 2 0 2 . 0 9 8 ~ 1 0 2 Z n 2 1 3 . 9 1 0 1 . 2 6 ~ 7 2 0 . 5 ~ 5 5 . 3 9 7 ~ 1 0 6 F e 2 4 8 . 3 1 0 1 . 2 6 ~ 7 2 2 ~ 2 0 2 . 1 9 8 ~ 1 0 2 M n 2 7 9 . 5 1 0 1 . 2 6 ~ 7 1 0 2 ~ 2 0 2 . 9 9 7 ~ 1 0 2 ,gl(uNmSOe-N_ϑCQ }vKm[, wQ g{US0_ I{Op0qQX[CQ }(W8^ĉ+Tϑ4ls^
Nr^pbKm[0
1 2 . 5 SYT-N_ϑCQ }vRg
1 2 . 5 . 1 7hTMRYti
яt^eg SYT uNSU\__ NTy{|A~Y;8 0 = '`T_0SYTv(ϑNNlv u;mo`o`vsQ0SYT uN
NNTSf[]N gsQ ؏N_ uirf[0vktf[I{ g@w[RvsQ|0SYTNNNwS{]NN( Sb uirSf[) _N]'Yvb/g/ec, Te_N:NwS{]NNcONeU\MbNSv gsO)Y0W;8 1 =0
YV[ gN:gg{tSYT uN YVߘToT{t@\0e,gS uw[SYT uNSeTNTGW[L%Ne^:W0bV1 9 8 7 t^1\]^N
0SYT[hQ'`ċN z^Tel 00
0SYTkS uhQ 0
0SYTkS uSf[hQhel 0 SYT-Nv^lTŔvKm[Ǒ(uSP[8T6eIQ1l v^ReQhhQv el ~ǏяNASt^v[ N Nv^lO(u0
SYT7hTvǑƖ V[hQ g%Ne5uopRs1 0 W IQ1&^[:N0 . 7 n m 0ۏ7hSOy:N2 0 L 0wXp)n^ z^:N: r^q)n^P b 1 2 0 !0A s 1 1 0 !, eaWGS)n1 5 s , Oce3 0 s ppS)n^P b 5 5 0 !0A s 1 2 0 0 !, eaWGS)n1 0 s , Oce3 0 s SP[S)n^:N2 3 0 0 !, eaWGS)n0 s , Oce2 s QS)n^2 7 0 0 !, eaWGS)n1 s , Oce3 s 0pQlAm2 5 0 m L . m i n - 1 SP[S6k\Pl0Kmϑe_:N\ؚ lopcb̀of (uhQf~l[ϑ0
elvhQPA s :N0 . 0 1 3 n g , P b :N0 . 0 1 0 n g , !hQf~~'`V:N0 ~ 0 . 1 m g . L - 1 R S D /f0 . 8 ~ 5 . 2 ( n = 6 ) RhV6es:N9 6 . 1 ~ 1 0 5 . 8 0
,glupOe^ؚ0|[^}Y, (uNmbvY0%{Qb0|^ 0Sm wmI{YySYT-N g[CQ }vKm[0
2 . IvKm[
yS~1 . 0 0 0 g 7hTnN2 5 m L kr{-N, ReQ3 m L SmH N O 3 xmlǏ Y0QN4ltm-NRpmS1 ~ 1 . 5 h , SQ
zQTReQ2 m L H 2 O 2 , ~~(W4ltm-NmS1 h , QtST[[1 0 m L , Te6RYՋBRzz}v;8 5 =0
Km[agN:N: lC d 2 2 8 . 8 n m zz_4gop5uAm7 . 5 m A IQ1&^[1 . 3 n m 0zzlAmϑ9 . 4 L . m i n
1 YNpAmϑ2 . 3 L . m i n
1 qphVؚ^7 . 5 m m 0Kmϑe_Z A A Kmϑe5 s 0(uhQf~l[ϑ0
,gl؏(uNSYT-N_ϑP b vKm[0
mS7hTela N[\7hTN4ltm-NSQ
zQTQRH 2 O 2 , N2N u'Yϑll\7hTQQ{Y0
3 . ;`^lvKm[
7hTSǑ(un_VAmml0PSmlbxmclYt ~2 0 S n C l 2 ؏SYt\ST`v^llS:NCQ }^l;8 2 =0
Ǒ(un_VAmmle S1 . 0 0 g Ջ7hnN2 5 0 m L W^pt-N, baReQ3 0 m L SmH N O 3 05 m L SyP[4l05 m L SmH 2 S O 4 Spe|sts0(W5up
NRpVAm2 h , nmHT_ĞbĞr, NQQ{
NSleQ1 0 m L 4l, ~~RpVAm1 0 m i n , QtS0ǏnmSm, nm[[5 0 m L 0
Ǒ(un_PSmle S~1 . 0 0 g Ջ7hnN1 0 0 m L %b_t-N, ReQ5 0 m g V 2 O 5 T7 m L SmH N O 3 0(Wltmb5upg
N_kpRp_l0S NQtS, R8 m L SmH 2 S O 4 , (W%b_tS>e N\stoe, N1 3 5 ~ 1 4 0 !)n^ N~~mv^(W_eeR\ϑH N O 3 , nmHTf݄~rbXj~r:Nbk0QtSTReQ\ϑ4l, ~~Rpnql~2 m i n NqvN O 2 , [[5 0 m L 0
Ǒ(uxmcle S1 . 0 0 g 7hTnN5 0 m L kr{-N, R5 m L SmH N O 3 01 m L H 2 O 2 , >e3 0 m i n T, (Wl4ltm-NRp~2 h , Q[)n, (u1 0 H 2 S O 4 [[5 0 m L 0,gl
NN+T!(7hT0
(u}l\^l}l&^eQSP[ShV Km[H g 2 5 3 . 7 n m v8TIQ^ Km[agNSSvQNe.s (uhQf~l[ϑ0
Yt1 g 7hT, hQP:N0 . 0 1 g . g
1 0
4 . vzzQSP[8T6elKm[uϑ^l
yS1 . 0 0 g 7hTnN5 0 m L kr{-N, Te\OՋBRzz}v NN, ReQ5 . 0 m L SmH N O 3 , 1 . 0 m L H 2 O 2 , Gd S0>en3 0 m i n T, (Wl4ltm-NRp2 h , Q[)n, (u1 0 H 2 S O 4 nm[[5 0 m L 0hQleQ1 0 0 m L }lSt-N, \}Yt^X, (ul\hVleQ2 . 0 m L 1 0 vS n C l 2 nm, /cGd1 0 0 s , Yn2 0 m i n 0hQnm_N c T7hekYt;8 6 =0
bS
NlSOleQKm^lNS^t-N, (W}lAmϑ6 0 m L . m i n
1 , /cGde1 0 0 s , s^ae2 0 m i n agN NKmϑH g 2 5 3 . 7 n m v\ؚ (uhQf~l[ϑ0
elvhQP:N0 . 0 6 g . k g - 1 Km[Sm^:N0 . 0 0 5 m g . L - 1 T0 . 0 2 0 m g . L - 1 7hT R S D ( n = 8 ) R+R:N3 . 6 0 T1 . 1 1 0s^GWV6es:N9 7 . 8 6 ( n = 5 ) 0
,glǑ(uY`vzzS7h, MQNx}l&^eQ[NhVv_c[, Rg~g3z[0Qnx, yr+RN'Yyb7hTRg0
Y7hT+T gYNI{ g:gՋBR, ^HQ(W4ltm
NS, TRmՋBRY7hT+T!(Y, ^Ǒ(unlVAmml0
5 SYT-NŔ+TϑKm[
SYT7hTSǑ(un_ml0r^nmlbxmclYt0
Ǒ(un_mle, S~1 . 0 0 ~ 2 . 0 0 g Ջ7hnNmS{-N, Rpe|sts, QR1 0 m L SmH N O 3 , Rpm, iR2 ~ 3 m L e, QtS0KNTReQ2 ~ 5 m L H C l O 4 , ~~Rpv^
NeGd S, Q}vp, m㉲m:NmĞrbernm, \m㉲mSm)0R1 m L ]S0QtST[[0R1 0 m L Ջ{-N0
Ǒ(ur^nmle, S~1 . 0 0 ~ 2 . 0 0 g Ջ7hnNtiWW-N, \kpbaRpvpS, QN5 0 0 ! NppS6 h ]S, QtSTSQ0TiWW-NReQ2 ~ 3 m L H N O 3 + H C l O 4 ( 3 + 1 ) mx, Te6RYՋBRzz}v, \_RpnmQQ}vp,
Nr^m0 gkX[p|, ^eR2 ~ 3 m L mx, S
Ym, v7hm:Nerb_Ğr0_kpRpSm)яr^, QtST[ϑly1 0 m L Ջ{-N0
Ǒ(uxmcle, yS~1 . 0 0 g 7hTnN1 0 m L b2 5 m L kr{-N, R2 m L SmH N O 3 T5 m L 3 0 H 2 O 2 Gd S, Nl4ltm-NRp2 h , QtST4l[[1 0 m L 0
S_7hT-N+T g'YϑyP[e \ՋmlySv-N, (W4ltm
NRpSr^, ReQ1 0 m L 7 m o l . L - 1 H C l n㉋k#n, (uI{ϑvM I B K S2 !k, Q(u5 m L 7 m o l . L - 1 H C l mM I B K B\, Tv^H C l nm, _evx0Y+T g'Yϑ˔I{, R\nmly1 0 0 m L Rmoe-N, R2 m L 2 0 gjxnmT1 n0 . 1 nIZ݄c:yBR, (u"l'lS(l( 1 + 1 ) nm:N~r0R2 m L 1 0 kxx(lnm, R4l0R3 0 m L , R2 m L 2 NYN(lWNkxN2ux( D D T C ) nm, >enpem i n , (u1 0 m L M I B K S3 m i n , RB\TKm[M I B K v-NvŔ0+T g'YϑA l 0C a I{yP[, R\nmly1 0 0 m L Rmoe-N, R2 m L 2 0 gjxnm, (u"l'lS(lp H 2 . 5 ~ 3 . 0 0R4l3 0 m L , R2 m L 2 !TTpNkxN2ux( A P D C ) nm, mTTYnGr;R, (u1 0 m L M I B K S3 m i n , \ g:gvlyy_{-N, N3 0 0 0 r . m i n - 1 Ny_5 m i n 0Km[M I B K v-NvŔ;8 2 =0
(ukp0qSP[8T6eIQ1lKm[ NhVagNSSvQNe.s NhQf~l[ϑ0
,glSKm7hT-NŔ gNO+Tϑ:N4 m g . k g - 1 0Y:N|{|7hT, R[[0R2 5 m L Ջ{-N, _ey_lmKmՋ
Nn Y0
6 . }v|-N_ϑŔvKm[
QnxyS0 . 2 0 0 0 g 7hTnN3 0 m L iWW-N, (u\ϑ4lmn, ReQ1 0 m L H F , (WNO)n5up
NRp v^
NeGdR, 7hTn:Nbk06qTReQ\ϑ4lT2 5 m L vSmH C l , ~~Rpl~, QtSTyeQ1 0 0 m L [ϑt-N, Te6RYzz}vnm;8 7 =0
Km[agN:N: lP b 2 8 3 . 2 n m , zz_4gop5uAm3 m A IQ1&^[0 . 2 n m 0YNpAmϑ3 L . m i n - 1 zzlAmϑ1 0 . 2 L . m i n - 1 qphVؚ^2 . 2 m m 0(uhQf~l[ϑ0!hQf~~'`V:N0 ~ 1 0 g / 5 0 m L 0
7hT-NT i O 2 (W9 8 N
N, xSǏ z-NT i f4l,
Nr^pbP b vKm[0(W+TP b ϑ:N5 . 3 0 g v7hT-N, ReQ5 0 0 g 0C a 2 + 0M g 2 + 0F e 3 + 0A l 3 + 0C o 2 + [Km[~geq_T0
,gl(uNX}v|RSYTSeN'lS( }ve) -N_ϑP b vKm[0
1 2 . 5 . 2 2 mSmSYr-N_ϑCQ }vKm[
1 mSm-NŔvKm[
QnxyS1 0 . 0 0 g mSm7hTnNr^QvtiWW-N, (W1 0 0 !p{-NRppяnvr, QN5 8 0 !ؚ)np-NppS~3 h , 7hT-Nv g:g(W,gppS[hQ0SQTQ[)n, ReQ2 m L H C l 1 + 1 , )npOiWWQir(n, ReQl4l8 m L , KNTQ[)n [[N1 0 m L [ϑt-N;8 8 =0ppS
N[hQb glm, S(u_ n~r^ǏnTKm[ TeZP2 *NN
Nvzz}vnm0
Km[agN:N: lP b 2 8 3 . 4 n m , zz_4gop5uAm6 m A IQ1&^[0 . 2 n m 0zzlAmϑ5 L . m i n - 1 YNpAmϑ0 . 9 L . m i n - 1 qphVؚ^1 5 m m 0ՋmcGSϑ4 . 2 m L . m i n - 1 0(uhQf~l[ϑ0
R S D /f4 . 9 6 ( n = 1 0 ) RhV6es:N9 9 . 7 ~ 1 0 1 . 3 0
7hT-NCQ }+TϑؚvN a 0Z n (WSm^:N1 e[~geq_T0
mSm-NP b +Tϑ N,(W1 g . g - 1 N N, (uH N O 3 + H C l O 4 nm, zz}vfb[Nclv^(uV O_(W O~cl-N NNel[sv^(ub:NS0
QI{N;9 5 =TT^(uؚ'`zz_4gop0ؚHeShV0w {YNp- zzlkp0qSP[8T6elKm[]NEx-NŔ, RgupOe^_0RN'Y'Y9eU0Ǒ(u Qۏ7hb/gSNMQ7hT-NF e 0A l I{(WSP[SǏ z-Nb_bv'lSir8TDw{X0SP[UcƖb/g;9 6 , 9 7 =0X ab/g;1 7 9 8 =0['lzzlYNpkp0q;9 9 =TQye;1 0 0 =x6RvؚupOe^qphVI{b/g^8^[(u, (W[E]\O-N_eeQؚSܑ-N (W1 6 0 !p{-NRp8 h 0QtSTSQ, NXZV lYNppog-NSяr^, R5 m L H N O 3 QSv=\H F , QR4l, яr^, (u4l zʑ2 5 m L [ϑt-N[[0RSϑ勶nmnN1 0 m L [ϑt-N, ReQ1 m L 1 0 m g . m L
1 NC a vC a ( N O 3 ) 2 nm\O:NWSO9eۏBR, (u4l z;R^;1 0 1 =0
Km[ewXp)n^ z^:N: r^q)n^1 2 0 !, Oce2 0 s ppS)n^1 3 0 0 !, Oce2 0 s SP[S)n^2 5 0 0 !, Oce4 s QS)n^2 6 0 0 !, Oce3 s 0SP[Se\Pl0(ulopcb̀of, \ؚKmϑe_ hQf~l[ϑ0
elvhQP:N4 n g . m L - 1 yr_(ϑ/f3 5 p g , R S D /f4 . 2 ( n = 7 ) RhV6es:N1 0 3 ~ 1 0 6 0!hQf~v~'`V:N0 ~ 0 . 4 m g . L - 1 0
,gl؏(uN g:gSTir-NuϑG e vKm[0
0 . 1 m o l . L - 1 N a O H eq_T, 'YN0 . 1 m o l . L - 1 vN a O H OWSO9eۏBRC a ( N O 3 ) 2 lmgQ00 . 1 ( v / v ) vH C l 0H 2 S O 4 0H C l O 4 N u%N͑ r^pb, 5 NQvH N O 3 eq_T, Vdk(WYtՋ7he[Ǒ(uH N O 3 0WSO9eۏBRbS O 4 2 - vr^pb0
2 'ltqplKm[dq-Nuϑ^l
Ǒ(u'ltqp H 2 S O 4 - K M n O 4 mTm:N8T6emYtdq7h, N/lSN!nm\O؏SBR, QSP[8T6elKm[^l;1 0 2 =0ySdq7h0 . 0 5 0 0 ~ 0 . 1 0 0 0 g , SeQ N\WWNHQjRb&^bvwb_n~-N( Te\Ozz}vՋ) , 6qT\vQ9Y>e(WV[N'lqpt^Xv
Nv\WM NQ{-N, n~bzQ(WY08TS1 0 . 0 m L H 2 S O 4 - K M n O 4 mTmMk:N: k1 0 0 m L nm-N+Tkxx1 0 m L , ؚ0x3 . 0 g nN'lqpt-N, vQelmntQX0>PeeQ'llpey, sSpqn~ ŏ \^XP['}^Xۏ'lqpt-N, PltP[, nm[\tS0qp[kT, \_/cGd6 ~ 7 m i n , QbnmleQ5 0 m L [ϑt-N, ReQ2 . 0 m L ( 1 + 1 ) H N O 3 , (u5 vxnmner, N4l[[08TSՋm2 5 . 0 m L nN5 0 m L l\hVQ, Q8T3 . 0 m L 1 0 ( +T1 0 vx) /lSN!nmSzzl1 2 . 0 m L ( Olm;`SOype:N4 0 . 0 m L ) , (WQlSzWY
NsN{, (u9_'|9Y9Y'}0gRp/cGd1 m i n T, sN{N8T6e`lޏc, ŏ \l\hVQlvRceQ8T6e`l-N Km[H g 2 5 3 . 7 n m v8TIQ^ (uhQf~l[ϑ0
Km[eop5uAm/f5 m A IQ1&^[0 . 4 n m 0
Km[vR S D /f3 . 7 ~ 1 2 . 5 , RhV6es:N9 0 ~ 1 0 5 0!hckf~v~'`V:N0 ~ 0 . 2 n g . m L - 1 0
l\hVQzzlϑ(W8 . 0 ~ 1 6 . 0 m L e, 8TIQ^'Y N3z[, zzlϑR'Y, 8TIQ^MNO07hT-NqQX[CQ }
Nr^pb, d\O_ 0{O, upOe^S͑s'`}Y, (uNdq-Nuϑ^lKm[0
3 xv-NxvcKm[
(W1_x'`N(-N, NbOW@x\O؏SBR\C u 2 + ؏S:NC u + , I - NC u + [ϑS^, ublm, RyT, lm~kxNkxxn, (WzzlYNpkp0q-NKm[ܔ, cBl_xv+Tϑ;1 0 3 =0
QnxyS1 0 . 0 0 0 0 g ^.UxvnN1 0 m L pog-N, R\ϑ4ln7hT0\nmleQ1 0 0 m L Rmoe-N, O!kReQ1 . 0 0 m L H 3 P O 4 05 . 0 0 m L 1 0 0 0 m g . L - 1 vK I hm01 0 . 0 0 m L C C l 4 nm, EQR/ca, YnRB\T\ g:gvleQS N1 0 0 m L Rmoe-N, v^ReQ0 . 5 0 m L 0 . 1 m o l . L - 1 N a 2 S O 3 01 0 . 0 0 m L 4lEQR/ca _S g:gv, 4lvleQ5 0 m L [ϑt-N, (u4l[[;R^0(W1 0 m L y_{-NO!kReQ0 . 5 0 m L 1 0 0 0 m g . L - 1 vC u S O 4 nm00 . 8 m L 1 0 0 0 m g . L - 1 vbOW@x02 . 0 0 m L 7hTnm00 . 5 0 m L 0 . 0 5 m o l . L - 1 vN2uxQnm, Gd S, Yn5 m i n , y_Ry, _S
NB\m0(u3 m L 4lmmlm, Q!ky_, _S4lv, ReQ0 . 3 m L 0 . 1 m o l . L - 1 vN a 2 S 2 O 3 nmn㉉lm, leQ2 5 m L [ϑt-N, mmy_{, Tv^mmmT(u4l[[;R^0
Km[agN:N: lC u 3 2 4 . 7 n m zz_4gop5uAm2 . 0 m A IQ1&^[0 . 2 n m 0YNpAmϑ1 0 0 L . h - 1 zzlAmϑ4 0 0 L . h - 1 qphVؚ^5 m m 0
elvyr_Sm^:N0 . 0 5 6 m g . L - 1 hQP:N0 . 0 1 9 m g . L - 1 R S D /f0 . 7 ( n = 7 ) RhV6es:N9 9 . 9 ~ 1 0 0 . 3 0!hQf~v~'`V:N0 ~ 8 0 0 m g . L - 1 0
,gl؏(uNNS }GrN+}܃-Nx+TϑKm[ (Wĉ[agN NqQX[CQ }
Nr^pb0
KmՋnmvx^[8TIQ^ gq_T N2uxQnmp H ~:N4 . 0 0
4 dq-NkxvcKm[
)R(uS O 4 2 - (WB a C r O 4 nm-NS[ϑnbcQC r O 4 2 - , Km[C r cKm[dq-Nkx09hnc
N TvRgBl, dq7hS c NelYt;1 0 4 =0
( 1 ) Km[hQkx
Sdq7h0 . 1 0 0 0 ~ 0 . 5 0 0 0 g NtiWW-NN~laSՋBR1 . 5 g mTGW S, Q(u1 . 0 g ~laSՋBR
Yv0\iWW(W8 0 0 ~ 8 5 0 !ؚ)np-NO)n1 . 5 ~ 2 h 0SQQtS, leQ3 0 0 m L pog-N, ReQ1 0 0 m L p4lEQRdb, NSB\['`n~NOǏn0nmQtST, (u4l[[2 5 0 m L [ϑt-N0
( 2 ) kxxvkxvKm[
Sdq7h0 . 1 0 0 0 ~ 0 . 5 0 0 0 g N1 0 0 m L pog-N, (u1 . 0 m L e4lYNnm0ReQ5 0 m L H C l ( 3 + 9 7 ) , (W5upg
NNO)nRp, _l3 0 m i n 0
zQT, (uSB\['`n~Ǐn1 0 0 m L pog-N nmQtST, (u4l[[2 5 0 m L [ϑt-N0
( 3 ) kxwkxvKm[
(W
N~H C l ( 3 + 9 7 ) YtǏvdq7hn#n-N, ReQH N O 3 ( 1 + 4 ) 4 0 m L , (W5upg
NNO)nRp, _l3 0 m i n , S N
zQ, Ǐn2 0 0 m L [ϑt-N[[0
yS7hm5 . 0 ~ 1 0 . 0 m L N5 0 m L pog-N, RH N O 3 ( 1 + 4 ) 2 n, >e(W5upg
NSяr^( nvr) 0S N
zQ, RH N O 3 ( 1 + 4 ) 5 n, p4l2 0 m L , N5upg
N_l3 ~ 5 m i n nvrir, R3 . 0 m L 2 ( +TH C l 2 v / v ) vB a C r O 4 `Jmm(W5upg
NNO)nRp, _l5 m i n TS N, >en2 ~ 3 h , ReQ2 . 0 m L (l4l( 1 + 1 ) , 5 . 0 m L e4lYN0Yn2 h , Ǐn, nmleQ1 0 0 m L [ϑt-N, lmN( 0 . 2 + 9 9 . 8 ) (l4lmm0(Wnm-NR1 2 . 0 m L H N O 3 ( 1 + 1 ) T1 0 m L Sm^:N3 0 0 g . L - 1 vN a 2 S O 4 nm, (u4l[[0
Km[eRg~l:NC r 3 5 8 . 1 n m , op5uAm5 . 0 m A , &^[^0 . 2 n m 0zzlAmϑ2 0 L . m i n - 1 , YNpAmϑ7 . 5 L . m i n - 1 qphVؚ^8 m m 0(uhQf~l[ϑ0
elvhQP:N1 1 0 - 4 m g . m L - 1 R S D /f0 . 9 ~ 3 . 1 ( n = 5 ) 0!hQf~v~'`V:N0 . 0 0 ~ 3 0 m g . m L - 1 ( Nkx) ,
qQX[CQ }
Nr^pbKm[0
5 wXPge-NkxvKm[
)R(uS O 4 2 - (WB a C r O 4 nm-NS[ϑnbcQC r O 4 2 - , Km[C r cKm[wXPge-Nvkx;1 0 5 =0yS N[ϑvՋ7hnN5 0 m L tiWW-N, ReQ NN~laSՋBRMkN a 2 C O 3 TM g O c1 : 2 NKNm S, (WvQ
NQvR~laSՋBR0(W8 0 0 !ؚ)np-N|pppeh , gk1 h Sb _p1 m i n , v0RՋ7h[hQR Q[)n0ReQ\ϑ4lly4 0 0 m L pog-N, (up4lmiWWQX N!k, v^eQpog-N( qQ1 5 0 m L ]S) , nql5 m i n , >PXǏnT(u5 0 m L p4lmm N!k0lmyeQoeT, Q(up4lmm8 ~ 1 0 !k, (Wnm-NReQZ^HT~r0Rpl~, ReQH C l ( 1 + 1 ) RN a 2 C O 3 v^Ǐϑ0 . 5 m L , nqlnm:N2 0 0 m L ]S, Q[)n, ReQ(l4lnm_~, leQ2 5 0 m L [ϑt-N[[0ƉS O 4 2 - +TϑS0 . 5 ~ 1 0 . 0 m L
Nnm( S O 4 2 -
NǏ3 0 0 g ) 0R2 5 m L kr{-N, Rx`Jmm2 . 0 m L , Gd S, >en5 m i n N
N0ReQC a C l 2 nmT( 1 + 1 ) (l4lT1 m L , e4lYN8 m L , R4l;R^, , >en1 h T(uba [ϑn~ǏneQ2 5 m L kr{-N0
(WlC r 3 5 7 . 9 n m Km[C r Km[agNSSvQNe.s NhQf~l[ϑ0elvhQP:N0 . 3 0 m g . L - 1 yr_Sm^:N0 . 3 1 m g . L - 1 , R S D /f2 . 8 ( n = 5 ) 0!hQf~v~'`V:N0 . 3 0 ~ 1 2 . 0 0 m g . L - 1 NS O 4 2 - 0
x`Jmm: 0 . 5 g xnN+TSmvx0 . 4 2 m L TQYNx1 4 . 7 m L v2 0 0 m L mTm-NC a C l 2 nmSm^:N1 0 0 0 m g " L - 1 NC a 2 + 0
,gl(uNkx+Tϑ'YN1 0 0 g " g - 1 vwXPgevKm[0
B a C r O 4 vn㉦^(Wp H < 1 1 e'Y (u(l4lnmvp H > 1 1 0
6 "lSirS ulvcKm[v-NRx
yS N[ϑRRxxv7hT, R4lnT[[1 0 0 m L b~H N O 3 - H C l O 4 ( 2 + 1 ) mxSH C l ( 1 + 9 ) mST[[0(W5 m o l . L - 1 H C l N(-N (u4 g L - 1 N a B H 4 S uRx"lSir;1 0 6 =0
Km[agN/fl:NS e 1 9 6 . 0 n m zz_4gop5uAm2 3 m A IQ1&^[0 . 5 n m 0qphVؚ^1 6 m m 0\ؚ[ϑ (ulopcb̀of hQf~l[ϑ0
elvR S D ( n = 7 ) :N1 . 3 T1 . 6 RhV6ess^GW:N9 6 . 3 0
N a B H 4 (W2 *NgKNQ3z[, K B H 4 3z['`]0v-NWSO
Nr^pbS e vKm[0
1 2 . 6 . 2 . 2 vtstSvQSe-N_ϑCQ }vKm[
1 wQ-NnQISŔvKm[
S^.UwQpe*N, (ummBRmQT, Q(u4lQm0r^q0(u]wQnxSOyv4 YNxln[hV, v}YT(W[)n N>en2 4 h , sS_Ջ7hnm;4 2 =0hQ|R_N(u4 YNx zʑM6R0
RgagN:N: lC d 2 2 8 . 8 n m P b 2 1 7 . 0 n m zz_4gop5uAmC d 8 m A P b 1 5 m A IQ1&^[0 . 3 3 n m 0YNpSR0 . 5 k g . c m - 2 YNpAmϑ3 . 5 L . m i n
1 zzlSR1 . 8 k g . c m - 2 zzlAmϑ1 4 L . m i n - 1 0qphVl2 0 ҉^0(uhQf~l[ϑ0
RgV:N: C d 0 . 0 ~ 1 . 0 m g . L - 1 P b 0 . 0 ~ 1 0 . 0 m g . L - 1 0
Nyb7hT8^bS1 0 *N7hT TeRg0傶nm-N_KmCQ }+Tϑؚe, S\7hT zʑblRqphVl҉egMNOKm[upOe^0
2 i_5ugIQO\Xst-NAvKm[
\i_5ugIQO\Xst|xb_\v~|r, ~mm0r^qTQnxySϑ7hTnNiWW-N, ReQ4l0"l lxT1 0 m L S\ϑkxx, 6qT\kpRpSr^0QtS, Rxn, yeQ2 5 0 m L [ϑt-N[[0\dknm zʑ N[
Ppe\O:N7hm, N2kKmCQ }r^pbyP[vmTm:NAmRl\v}m;1 0 7 =0
AmRl\eǑ7he1 0 s ۏ7he1 0 s ۏ7hϑ3 0 l }mAmϑ1 . 8 m L . m i n - 1 0S^{^K 0M g TF e 2 0 c m N a TC a b3 0 c m 0Km[agN:N: lK 7 6 6 . 5 n m N a 5 8 9 . 6 n m C a 4 2 2 . 7 n m M g 2 8 5 . 2 n m F e 2 4 8 . 3 n m zz_4gop5uAmN a :N8 m A , vQ[CQ }:N1 0 m A 0zzlAmϑGW:N4 . 5 L . m i n - 1 YNpAmϑF e TM g :N0 . 2 L . m i n - 1 , vQ[:N0 . 8 L . m i n - 1 0qphVؚ^K :N5 . 0 m m N a TC a :N7 . 0 m m M g TF e :N6 . 0 m m 0(uhQf~l[ϑ0
elvhQPK /f0 . 1 0 m g . L - 1 , N a /f0 . 0 3 m g . L - 1 , C a /f0 . 2 5 m g . L - 1 , M g /f0 . 0 4 m g . L - 1 F e /f0 . 0 5 m g . L - 1 0!hQf~~'`VK :N1 . 0 ~ 1 0 . 0 m g . L - 1 N a 0 ~ 3 . 2 m g . L - 1 C a 1 0 . 0 ~ 2 6 . 0 m g . L - 1 M g 0 . 0 4 ~ 2 . 2 m g . L - 1 F e 0 . 5 ~ 1 5 . 5 m g . L - 1 0RhV6esTCQ }GW(W9 0 ~ 1 1 0 KN0
Km[evlaNy:N( 1 ) @b(uՋBRGW:NO~~, NQ\zz}v 1 0 , dkenm-NǏϑvM g 2 + N8 - WUIUb_blm, nbcQvM g 2 + OYu(Wnm-N0r^ǏnQlm, (WSP[8T6eIQ1N
NKm[nm-NvM g 2 + , sSScKm[I n 3 + +Tϑ;1 0 9 =0
yS7hT0 . 2 5 0 0 g nNMiWW-N, (W6 5 0 !)n^ Nq1 5 m i n , QtSTleQ3 0 0 m L pog-N, (up4lxmSqirv^v=\H 2 O 2 , QtSTǏn, _Snm, (u5 0 g . L - 1 N a O H nmblmm0RSegpog-N, (u1 0 m L ( 1 + 1 ) H C l n㉉lm, ly0R2 5 0 m L [ϑt-N[[0S2 m L 7hmN5 0 m L \pog-N, ReQ3 ~ 4 m L 5 m o l . L - 1 "lnxnm, S
Yr^$N N!k, QR1 0 m L 5 m o l . L - 1 "lnx)npnv{|0QtSTR\K I Sx~vN a 2 S O 3 dbnmHTmĞr, ly1 2 5 m L oe-N, R1 5 m L YNxNo/ca1 m i n , RB\T_S4lv, g:gv(u1 0 m L ( 1 + 1 ) H C l T3 ~ 5 nH 2 O 2 SS$N!k, 6eƖ4lvN5 0 m L pog-N Rpяr^, R1 m L SmH 2 S O 4 Rp}vpQ=\, QR2 m L ( 1 + 1 ) vx, )npn0ReQ4 m L A- 8 - WUIUnm, 3 m L 9 5 YN, (u(l4lp H :N6 . 5 , db5 m i n , ~~nR(l4l1 4 m L , ly5 0 m L [ϑt-N, [[T>en1 5 m i n , r^Ǐn0R\pog-N,
N:gKm[0
elvyr_Sm^NI n 3 + :N0 . 0 2 m g . L - 1 , R S D /f1 . 4 7 T0 . 5 7 , RhV6es:N9 9 0!hQf~v~'`V:N0 ~ 2 . 5 m g . L - 1 NI n 3 + 0
ReQ\ϑYN, /f:NNX'Y8 - WUIUn㉦^0~ST7hT-NqQX[yP[
Nr^pbKm[0
A- 8 - WUIUnmv6RY: S0 . 1 2 0 g 'lSAR( 1 + 1 ) vx5 m L n, zʑ3 0 0 m L , ReQ5 5 m L 8 - WUIUnm( 2 ) , Rp0R7 0 ~ 8 0 !, S N, db NnR(l4lnmmJm, QǏϑ(l4l1 0 ~ 1 2 m L , , db1 0 m i n , >en4 0 m i n , Ǐn, mmnmeĞr, (u5 5 m L QYNxn㉉lm, ly5 0 0 m L [ϑt-N[[0
3 'lS-NvKm[
S O 4 2 - Sb6RSP[v5uy e SR5uyb6RBR0(WH 2 S O 4 - ( N H 4 ) 2 S O 4 N(-NS
NRyvcNkp0qSP[8T6elKm['lST'lS-Nv;1 1 0 =0N a < 0 . 1 vՋ7h, (uhQReQlKm[ N a e"0 . 1 vՋ7h, R(uhQf~l0
( 1 ) hQReQl0yS0 . 1 0 0 0 00 . 5 0 0 0 T1 . 0 0 0 g Ջ7h, nNr^qv1 0 0 m L pog-N, R+RReQ3 05 01 0 m L H 2 S O 4 T2 03 05 g ( N H 4 ) 2 S O 4 , v
Nhbv, RpnnmnNT yeQ5 0 m L b1 0 0 m L [ϑt-N[[0RSnm3 NN3 *N1 0 0 m L [ϑt-N, RS
PpeSQNO g~nm-NN a vSm^:N0 . 2 m g . L - 1 ]S0(WvQ-N2 *N[ϑt-N, R+RReQ2 . 0 04 . 0 m L Sm^:N1 0 m g . L - 1 vhm, (u4l z;R^0
( 2 ) hQf~l0ySՋ7h0 . 1 0 0 0 g nNpr^v1 0 0 m L pog-N, ReQ3 m L H 2 S O 4 T2 g ( N H 4 ) 2 S O 4 , Rpn, _nmnNT, yeQ1 0 0 m L [ϑt-N, O g~nm-NN a Sm^c6R(W0 . 2 ~ 1 . 0 m g . L - 1 Q, [[0
Km[agN:N: lN a 5 8 9 . 0 n m zz_4gop5uAm2 m A &^[^0 . 1 n m 0qphVؚ^1 0 m m YNpAmϑ1 . 2 L . m i n - 1 zzlAmϑ6 . 0 L . m i n - 1 0
elvR S D (WN a +Tϑ0 . 0 5 e/f3 . 9 , +Tϑ0 . 7 e/f1 . 3 0RhV6es:N9 4 ~ 1 0 6 0
Z r O 2 bH f O 2 v+TϑNON0 . 5 g . L - 1 e, [Km[eq_T ؚN0 . 5 g . L - 1 e, eu g r^pb0
4 0lSm-NŔvKm[
(Wcё0lSm-N 8^RC a O , p H ~:N1 2 , ŔN[ P b ( C N ) 4 ] 2 - ~4yP[X[(W0(WhQ]\Onm-N ReQ5 m L gjxT5 m L +TK C N nm, NMQ(Wx'`agN NŔvlm;1 1 1 =07hm-N_NReQ5 m L gjx0
Km[agN:N: lP b 2 8 3 . 3 n m , zz_4gop5uAm1 m A IQ1&^[0 . 4 n m 0YNpAmϑ3 L . m i n - 1 zzlAmϑ1 3 L . m i n - 1 qphVؚ^7 . 5 m m 0(uhQf~l[ϑ0
elvR S D :N1 . 8 ( n = 1 0 ) 0
7hm-N8^vF e 3 + 0C a 2 + 0C u 2 + 0Z n 2 + 0A l 3 + 0A g + 0P t 2 + 0P d 2 + I{yP[(WkKQ~[Km[er^pb0
Yt7hTe xSՋ7hnm, \>eQgRkH C N lSO0
+TK C N nmM6R: S4 g C a O , R5 0 0 m L 4lnv^Ǐn, nm-NR3 g K C N , (u4l z1 0 0 0 m L 0
laNy0lSir gk d\ONXTR_u[[[v[hQd\Oĉ z ǑS[hQ2bce ON[hQ0(uǏv+T0lSir^m(uN(u[hVPX[TYt
N_OceQ N4lS00lSirՋBRT7hTNN #O{0
5 Z n S : M n NAm5uSIQO\-N 0vKm[
\@ gZ n S : M n vst}Gr, r^qR`͑T, Qnxyϑ, 6qT(W+}Yop NRp, nRQnvx( 1 + 1 ) , )R(umSOv6q _Rn7hT, _kxS"llSO8QT, (u4lQm}Gr, v^6eƖQmmNwpog-N, Q\e}Grr^qR`͑Tyϑ, ]y, 1 9 9 0 ,{ASz
1 2 Ng[!j, O~-N{. SP[8T6eSSP[gIQIQ1Rg. SN: yf[QHr>y, 2 0 0 0 . 2 7 2 ,{kQz,{V
1 3 Y['Ywm, s\Y, Ğ,gz. RgNhV. 1 9 9 9 , ( 2 ) : 5 3
1 4 [Ual_, Nq. Slё^\CQ }hQir(x6R. : UO.^s^;N. _ϑCQ }xvzۏU\( ,{ N) . SN: -NVgNQHr>y, 1 9 9 9 , 2 2 1
1 5 RzL lf[o ly. tSh- Sf[RQ. 2 0 0 1 , 3 7 ( 5 ) : 2 2 0
1 6 \, RzL, kee. QёRg. 2 0 0 1 , 2 1 ( 1 ) : 2 4
1 7 u1r N. RgSf[. 2 0 0 0 , 2 8 ( 3 ) : 3 3 3
1 8 s~kS, OKf. kp0qSP[8T6eIQ1lKm[mnl-NuϑŔMTA. : Ng Ne;N. _ϑCQ }xvzۏU\( ,{V ) .
Nwm: ,{NQ;S'Yf[QHr>y, 2 0 0 1 . 9 2
1 9 RzL, Y[zNS, l~s^. wlS]. 2 0 0 0 , 2 9 ( 6 ) : 4 4 6
2 0 RzL,
Oys, u=NI{. wlS]. 2 0 0 0 , 2 9 ( 3 ) : 2 1 1
2 1 l%f*t, ߏ!X, ef_. SN^'Yf[f[b( 6qyf[Hr) , 1 9 9 5 , 3 1 ( 2 ) : 2 3 4
2 2 ^, Q~, NgO. RgNhV. 1 9 9 8 ( 4 ) : 3 6
2 3 ёs, HN, Y[pg. wlS]. 2 0 0 0 , 2 9 ( 7 ) : 5 2 4
2 4 ^8l)P _\s. NWSS]. 2 0 0 5 , 3 2 ( 1 ) : 3 3
2 5 hge u. q\ NS]. 2 0 0 4 , 3 3 ( 6 ) : 3 9
2 6 jl fN. IQ1f[NIQ1Rg. 1 9 9 1 , 1 1 ( 1 ) : 6 8
2 7 sQ[fk. tSh( Sf[RQ) . 1 9 9 0 , 2 6 ( 4 ) : 2 3 0
2 8 _Mg. wlS]. 1 9 9 5 , 2 4 ( 1 2 ) : 8 8 5
2 9 _Ώ z_ Z/c\I{. wlS]sXOb. 2 0 0 4 , 2 7 ( 4 ) : 5 4
3 0 9\s%Z Ng=NNS -NNS. q\S]. 2 0 0 5 , 2 5 ( 3 ) : 2 8
3 1 Ny, 1 9 9 4 . 4 5 5 3 1 2 8 2 0 7 3 2 4 5 5 8 7 2 9
3 5 z_, hg_pg, s }pQI{. S] uNNb/g. 2 0 0 1 , 8 ( 1 ) : 3 6
3 6 [,gs, R8l, NNn. wlp6RNS]. 1 9 9 9 , 3 0 ( 1 ) : 4 7
3 7 Yl. mnl. 2 0 0 0 , 1 5 ( 2 ) : 5 4 .
3 8 TN f[, k/T O. wlS]b/gveۏU\[ J ] S]ۏU\. 2 0 0 3 , 2 2 ( 2 ) : 1 0 9 ~ 1 1 2
3 9 ёley, g[{. SP[IQ1Rg. fkIl: -NV0W('Yf[QHr>y, 1 9 9 2 . 3 6 7
4 0 B . W e l z W. Ng[q, H `, I{ы. SP[8T6eIQ1l. SN: 0W(QHr>y, 1 9 8 9 , 4 8 6 , 4 8 7
4 1 l!`}, UONS q, hgxUmW. wXpSP[8T6eRIQIQ^l. SN: SP[QHr>y, 1 9 8 9 . 4 2 8 4 2 9
4 2 SN,{NIQf[NhVS`b[. SP[8T6eIQ1Rgel . SN: SN'Yf[QHr>y, 1 9 8 1 . 1 0 8 1 4 8 1 5 3
4 3 NO u, _)RtQ. IQ1[[. 1 9 9 3 , 1 0 ( 5 ) : 4 6
4 4 HSNy. \wKmՋ. 1 9 9 1 , 1 0 ( 4 ) : 2 9 1
4 5 hg_n. wlS]. 2 0 0 1 , 3 0 ( 8 ) : 6 3 5
4 6 ( e) e:g^(ukrRgYXTO. _, bʃ, Ng8lNSы. CQ }[(uIQ^Rg. l3: [yf[b/gQHr>y, 1 9 8 8 . 4 3 8 9 5 1
4 7 ёs|j, ёo, &{U\f. tSh- Sf[RQ. 2 0 0 1 , 3 7 ( 3 ) : 1 2 1
4 8 ucg, ll, R[. IQ1[[. 1 9 9 7 , 1 4 ( 2 ) : 5 9
4 9 ёs|j, N{[, RQO. tSh- Sf[RQ, 2 0 0 0 , 3 6 ( 9 ) : 4 1 0
5 0 k[~g H_[ [zeI{. -NV/lx. 2 0 0 2 , ( 1 1 ) : 3 6
5 1 s=Ns, }vss. IQ1f[NIQ1Rg. 1 9 9 8 , 1 8 ( 5 ) : 6 0 6
5 2 _m , Oe. Sf[] z^, 1 9 9 9 , ( 6 ) : 4 5
5 3 \8lN. yryaj6RT. 1 9 9 7 , 1 8 ( 3 ) : 4 1
5 4 hTj, ؚ=N, N. )Y6qajsN-N_ϑCQ }Rgv7hTYtelxvz. : UO.^s^;N, _ϑCQ }xvzۏU\( ,{ N) . SN: -NVgNQHr>y, 1 9 9 9 . 2 6 5
5 5 Yf u O h sfNOI{. IQ1f[NIQ1Rg. 2 0 0 3 , 2 3 ( 2 ) : 3 7 7
5 6 0us, uhMb, Hg. IQ1[[. 1 9 9 7 , 1 4 ( 4 ) : 5 3
5 7 gSf8. IQ1NhVNRg. 2 0 0 1 , ( 4 ) : 3 6
5 8 Ngss, [`{. SP[8T6eRg^(uKbQ. SN: yf[b/gQHr>y, 1 9 9 0 . 2 7 7
5 9
Ockn, Y[i_N. IQ1f[NIQ1Rg. 1 9 9 8 , 1 8 ( 6 ) : 7 1 1
6 0 [Sfe. |~wlS]. 1 9 9 3 , ( 4 ) : 5 6
6 1 s~`l. lWSS]. 2 0 0 1 , ( 5 ) 3 3
6 2 upQ. |~wlS]. 1 9 9 7 , ( 2 ) : 5 5
6 3 ~)Y, hTwms, H=ޘ. Tb~~]N. 1 9 8 5 ( 4 ) : 2 9
6 4 1g*ml. wlS]PSBRW@xwƋ. SN: -NVwSQHr>y, 1 9 9 5 . ,{Nz ,{mQz
6 5 R ^'\I{W. ]NPSBRRgKmՋh_. SN: pR]QHr>y, 1 9 9 0 . ,{]Nz
6 7 l. wlp6RNS]. 1 9 9 8 , 2 9 ( 9 ) : 5 1
6 8 NgsO. wlS]. 1 9 9 8 , 2 7 ( 8 ) : 5 9 3
6 8 hg[, ~O, 4Te. wlS]Rgel( R I P P Ջel) . SN: yf[QHr>y, 1 9 9 0 . 3 1 6 3 2 3 3 2 6 3 3 3 3 3 9
6 9 Rh. wlS]. 1 9 9 7 , 2 6 ( 1 0 ) : 6 9 4
7 0 ёs. wlS]. 1 9 9 9 , 2 8 ( 9 ) : 6 2 6
7 1 NU\, _of, 1gs. irtKmՋ. 2 0 0 0 , ( 2 ) : 2 6
7 2 hg#kc. RgKmՋb. 1 9 8 6 , 5 ( 5 ) : 5 9
7 3 ёs. wlS]. 1 9 9 5 , 2 4 ( 6 ) : 4 2 2
7 4 _~~ q^CQ. tSh- Sf[RQ, 2 0 0 1 , 3 7 ( 1 ) : 2 9
7 5 Hqe, Hqf. wlS]. 1 9 9 9 , 2 8 ( 2 ) : 1 1 6
7 6 _^^. IQ1f[NIQ1Rg. 1 9 8 7 , 7 ( 4 ) : 5 5
7 7 旐t, _[_, qI{. RgSf[. 2 0 0 0 , 2 8 ( 3 ) : 3 8 8
7 8 R^t$. SP[8T6elKm[D S D x-Nv_ϑ. : _g ;N. _ϑCQ }xvzۏU\( ,{ N) . SN: Sf[]NQHr>y, 1 9 9 5 . 3 9 0 ~ 3 9 1
7 9 egQh. US]. 1 9 9 8 , 2 7 ( 4 ) : 3 5
8 0 sWINW. SYT- St Me uN]z. SN: Sf[]NQHr>y, 1 9 9 9 . 2
8 1 FIQ]. |~S], 1 9 9 9 , 1 6 ( X
R) : 1
8 2 -NVhQQHr>y,{ N[. SYThQGl. SN: -NVhQQHr>y, 1 9 9 6 . 1 0 1 4 1 1 4 9
8 3 ec;N. SP[8T6eIQ1l(WkS uh-Nv^(u. SN: SN'Yf[QHr>y, 1 9 9 1 . 1 4 8 1 8 8
8 4 ؚ#k. IQ1[[. 1 9 9 6 , 1 3 ( 4 ) : 2 3
8 5 Ngh, ![, fN
I{. ^Xfkp0qSP[8T6eIQ1^(uKbQ. SN: 0W(QHr>y, 1 9 9 6 . 1 0 7
8 6 ёo. e(uSf[]N. 1 9 9 5 , ( 5 ) : 2 9
8 7 NgShQ. S] uNNb/g. 2 0 0 1 , 8 ( 4 ) : 3 0
8 8 Ws^, R[^. tSh- Sf[RQ. 1 9 9 8 , 3 4 ( 1 0 ) : 4 6 9
8 9 ^t#Z. IQ1[[. 1 9 9 7 , 1 4 ( 6 ) : 4 1
9 0 e&OW. AmRl\Rg. SN: yf[QHr>y, 1 9 9 9 , ,{kQz,{V
9 1 _mdW e&O. RgSf[. 1 9 9 9 , 2 7 ( 7 ) : 8 4 5
9 2 e&O. RgNhV. 2 0 0 1 , ( 2 ) : 1
9 3 Q. sNNhV. 2 0 0 1 , ( 2 ) : 4
9 4 R Ns. SdqQy7hTMRYtelvk. : Ng Ne;N. _ϑCQ }xvzۏU\( ,{V ) .
Nwm: ,{NQ;S'Yf[QHr>y, 2 0 0 1 . 1 0 6
9 5 Q, qT-N, R*mU_. RgՋ[. 1 9 9 7 , 1 6 ( 4 ) : 6 4
9 6 RzL, ёs. IQ1[[. 1 9 9 3 , 1 0 ( 5 ) : 1 6
9 7 uۏl, _e, hg. RgSf[. 1 9 9 2 , 2 0 ( 6 ) : 7 4 1
9 8 Y[Ile, HpQʃ, Y[^l. IQ1f[NIQ1Rg. 1 9 9 8 , 1 8 ( 5 ) : 5 9 7
9 9 8lT, O~-N, lIQckI{. RgSf[. 1 9 9 0 , 1 8 ( 1 ) : 7 2
1 0 0 Qye, hgs4t. IQ1f[NIQ1Rg. 1 9 9 8 , 1 8 ( 6 ) : 7 3 1
1 0 1 Yёs, 8ln. RgKmՋb. 1 9 9 0 , 9 ( 3 ) : 3 5
1 0 2 "^p. tSh- Sf[RQ. 1 9 9 7 , 3 3 ( 5 ) : 2 1 0
1 0 3 Y[Ile, Y[zfl, __:_. IQ1f[NIQ1Rg. 2 0 0 0 , 2 0 ( 4 ) : 5 3 7
1 0 4 "^p, 4TV. tSh- Sf[RQ. 2 0 0 0 , 3 6 ( 8 ) : 3 5 0
1 0 5
Oee, _P[R, 4Tn2m. RgSf[. 2 0 0 0 , 2 8 ( 1 0 ) : 1 3 2 0
1 0 6 9N, _e Z. tSh- Sf[RQ. 1 9 9 9 , 3 5 ( 3 ) : 1 3 5
1 0 7 z^^, hTŖ=N, WfNI{. tSh- Sf[RQ. 1 9 9 4 , 3 0 ( 9 ) 1 4 4
1 0 8 \gۏey, sё%f, HkI{. IQ1[[, 2 0 0 1 , 1 8 ( 1 ) : 7 1
1 0 9 RsN, [BhpQ, HFQNYI{. Sf[Rgϑ, 2 0 0 0 , 9 ( 2 ) : 3 0
1 1 0 R, υUae. RgSf[. 1 9 9 9 , 2 7 ( 1 1 ) : 1 2 8 4
1 1 1 fOpQ, hgtQfk. \wKmՋ. 2 0 0 1 , 2 0 ( 4 ) : 3 0 9
1 1 2 NeIQ. tSh- Sf[RQ. 1 9 9 8 , 3 4 ( 4 ) : 1 4 7
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